A Novel Palladium-Catalyzed Cross-Coupling of Thiomethylated Alkynes with Functionalized Organozinc Reagents

Laurin Melzig; Jeremy Stemper; Paul Knochel

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A Novel Palladium-Catalyzed Cross-Coupling of Thiomethylated Alkynes with Functionalized Organozinc Reagents

机译：具有官能化有机夹试剂的新型钯催化的硫代甲基化炔烃的交联

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A range of methylthio-substituted acetylenes undergo smooth palladium-catalyzed cross-coupling reactions with functionalized aryl-, heteroaryl-, and alkylzinc reagents using the Pd(OAc)_2/DPE-Phos catalytic system at 25 or 50 癈 without the need for copper salts.

机译：一系列甲硫基取代的乙炔，使用Pd（OAC）_2 / DPE-PHOS催化系统在25或50℃下使用官能化芳基 - ，杂芳基和烷基锌试剂经历光滑的钯催化的交叉偶联反应，而无需铜盐。

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来源
《Synthesis: International Journal of Methods in Synthetic Organic Chemistry 》 |2010年第12期| 共7页
作者
Laurin Melzig; Jeremy Stemper; Paul Knochel;
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作者单位

Department Chemie Ludwig-Maximilians-Universitat Munchen Butenandtstr. 5-13 Haus F 81377 Munchen Germany;

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原文格式 PDF
正文语种 eng
中图分类化学 ;
关键词
alkynes; cross-coupling; organometallic reagents; palladium; zinc;

机译：alkynes;交叉耦合;有机金属试剂;钯;锌;

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1. A Novel Palladium-Catalyzed Cross-Coupling of Thiomethylated Alkynes with Functionalized Organozinc Reagents [J] . Laurin Melzig, Jeremy Stemper, Paul Knochel Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2010 ,第12期

机译：新型钯催化的硫代甲基化炔烃与功能化有机锌试剂的交叉偶联
2. A Novel Palladium-Catalyzed Cross-Coupling of Thiomethylated Alkynes with Functionalized Organozinc Reagents [J] . Laurin Melzig, Jeremy Stemper, Paul Knochel Synthesis: International Journal of Methods in Synthetic Organic Chemistry . 2010 ,第12期

机译：具有官能化有机夹试剂的新型钯催化的硫代甲基化炔烃的交联
3. Room Temperature Cross-Coupling of Highly Functionalized Organozinc Reagents with Thiomethylated N-Heterocycles by Nickel Catalysis [J] . Laurin Melzig, Albrecht Metzger, Paul Knochel The Journal of Organic Chemistry . 2010 ,第6期

机译：镍催化在室温下将高官能度有机锌试剂与硫代甲基化的N-杂环偶联
4. Cross-coupling Reaction of Alkyl Halides with Organozinc and Grignard Reagents Using Bis-dienes as Additives [C] . Jun Terao, Hideyuki Watanabe, Aki Ikumi, Symposium on Organometallic Chemistry . 2003

机译：烷基卤化物与有机锌和格氏试剂的交叉偶联反应使用双二烯作为添加剂
5. PALLADIUM-CATALYZED CROSS COUPLING INVOLVING PROXIMALLY HETEROFUNCTIONAL REAGENTS (PALLADIUM, CROSS-COUPLING). [D] . LUO, FEN-TAIR. 1984

机译：涉及近位异功能试剂（钯，交叉偶联）的钯催化交叉偶联。
6. Organozinc Chemistry Enabled by Micellar Catalysis. Palladium-Catalyzed Cross-Couplings between Alkyl and Aryl Bromides in Water at Room Temperature [O] . Christophe Duplais, Arkady Krasovskiy, Bruce H. Lipshutz -1

机译：有机锌化学启用胶束催化。烷基和芳溴化物之间的钯催化交叉偶联在常温水中
7. Transition-Metal Catalyzed Cross-Coupling Reactions of Functionalized Organometallic Reagents, Nickel-Catalyzed Amination of Aryl Chlorides and Preparation and Reactions of Organozinc Reagents [O] . Manolikakes Georg 2009

机译：过渡金属催化的功能化有机金属试剂的交叉偶联反应，镍催化的芳酰氯胺化反应和有机锌试剂的反应

A Novel Palladium-Catalyzed Cross-Coupling of Thiomethylated Alkynes with Functionalized Organozinc Reagents

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