Oxidation of 1,4-disubstituted-1,2,3-triazoles with H2O2-CF3CO2H: efficient synthesis of 1,2,3-triazole 3-oxides

Gonzalez-Mojica Norberto; Almazan-Sanchez Leticia; Garcia-Torres Jesus G.; Santana-Martinez Ivette; Martinez-Otero Diego; Sanchez-Carmona Miguel A.; Cuevas-Yanez Erick

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Oxidation of 1,4-disubstituted-1,2,3-triazoles with H2O2-CF3CO2H: efficient synthesis of 1,2,3-triazole 3-oxides

机译：用H 2 O 2-CF 3 CO 2H氧化1,4-二取代的-1,2,3-三唑：1,2,3-三唑3氧化物的有效合成

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摘要

A collection of 1,2,3-triazole-3-oxides was obtained from oxidation of the corresponding 1,4-disubstituted-1,2,3-triazoles mediated by a H2O2-CF3CO2H system through a simple protocol in good yields showing high efficiency.

机译：1,2,3-三唑-3-氧化物的收集是通过通过简单的方案介导的相应的1,4-二取代-1,2,3-三唑的氧化，以良好的产量显示出高效率。

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《Synthetic Communications》 |2019年第8期|共9页
作者
Gonzalez-Mojica Norberto; Almazan-Sanchez Leticia; Garcia-Torres Jesus G.; Santana-Martinez Ivette; Martinez-Otero Diego; Sanchez-Carmona Miguel A.; Cuevas-Yanez Erick;
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Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

Univ Autonoma Estado Mexico Ctr Conjunto Invest Quim Sustentable UAEM UNAM Carretera Toluca Atlacomulco Km 14-5 Toluca 50200 Estado De Mexic Mexico;

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正文语种 eng
中图分类有机化学;
关键词
Hydrogen peroxide; oxidation; trifluoroacetic acid; 1; 2; 3-triazole 3-oxides;

机译：过氧化氢;氧化;三氟乙酸;1;2;3-三唑3氧化物;

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专利

1. Oxidation of 1,4-disubstituted-1,2,3-triazoles with H2O2-CF3CO2H: efficient synthesis of 1,2,3-triazole 3-oxides [J] . Gonzalez-Mojica Norberto, Almazan-Sanchez Leticia, Garcia-Torres Jesus G., Synthetic Communications . 2019,第5a8期

机译：用H 2 O 2-CF 3 CO 2H氧化1,4-二取代的-1,2,3-三唑：1,2,3-三唑3氧化物的有效合成
2. 'Green' synthesis of 1,4-disubstituted 5-iodo-1,2,3-triazoles under neat conditions, and an efficient approach of construction of 1,4,5-trisubstituted 1,2,3-triazoles in one pot [J] . Wang Dong, Chen Si, Chen Baohua Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第51期

机译：在纯净条件下“绿色”合成1,4-二取代的5-碘-1,2,3-三唑，以及在一个锅中构建1,4,5-三取代的1,2,3-三唑的有效方法
3. One-pot synthesis of 1,4-disubstituted 1,2,3-triazoles via Huisgen 1,3-dipolar cycloaddition catalysed by SiO2-Cu(I) oxide and single crystal X-ray analysis of 1-benzyl-4-phenyl-1H-1,2,3-triazole [J] . Gupta Manjulla, Gupta Monika, Paul Satya, Monatshefte fur Chemie . 2015,第1期

机译：SiO2-Cu（I）氧化物催化的Huisgen 1,3-偶极环加成反应一锅法合成1,4-二取代的1,2,3-三唑和1-苄基-4-苯基-的单晶X射线分析1H-1,2,3-三唑
4. Copper(II) Triflate as a Double Catalyst for the One-Pot Click Synthesis of 1,4-Disubstituted 1,2,3-Triazoles from Benzylic Acetates [C] . Eiji Shimizu, Satoshi Kikuchi, Shin-ichi Fnkuzawa Symposium on Organometallic Chemistry . 2007

机译：铜（II）作为单罐的双催化剂，单击1,4-二取代的1,2,3-三唑的双催化剂，从苄基乙酸盐中键合
5. Antibacterial agents: 1,4-disubstituted 1,2,3-triazole analog of the oxazolidinone. [D] . Acquaah-Harrison, George. 2010

机译：抗菌剂：恶唑烷酮的1,4-二取代1,2,3-三唑类似物。
6. 1,4-Disubstituted 1H-1,2,3-Triazole Containing Peptidotriazolamers: A New Class of Peptidomimetics With Interesting Foldamer Properties [O] . David C. Schröder, Oliver Kracker, Tanja Fröhr, 1970

机译：1,4-二取代的1H-1,2,3-三唑类含有肽三唑酰胺类：具有有趣的Foldamer性质的新型拟肽
7. CoFe2O4/Cu(OH)2 magnetic nanocomposite: an efficient and reusable heterogeneous catalyst for one-pot synthesis of β-hydroxy-1,4-disubstituted-1,2,3-triazoles from epoxides [O] . Ronak Eisavi, Asmar Karimi 2019

机译：COFE2O4 / Cu（OH）2磁性纳米复合材料：一种高效且可重复使用的非均相催化剂，用于单钾合成β-羟基-1,4-二取代的-1,2,3-三唑的氧化环氧化物
8. Synthesis, Characterization, and Structural Investigations of 1-amino-3-Substituted- 1,2,3-Triazolium Salts, and a New Route to 1-substituted-1,2,3- triazoles [R] . Kaplan, G. , Drake, G. , Tollison, K. , 2004

机译：1-氨基-3-取代-1,2,3-三唑盐的合成，表征和结构研究，以及1-取代-1,2,3-三唑的新途径

Oxidation of 1,4-disubstituted-1,2,3-triazoles with H2O2-CF3CO2H: efficient synthesis of 1,2,3-triazole 3-oxides

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