Pd/Cu-Catalyzed Domino Cyclization/Deborylation of Alkene-Tethered Carbamoyl Chloride and 1,1-Diborylmethane

Zhang Chenhuan; Wu Xianqing; Wang Chenchen; Zhang Chengxi; Qu Jingping; Chen Yifeng

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Pd/Cu-Catalyzed Domino Cyclization/Deborylation of Alkene-Tethered Carbamoyl Chloride and 1,1-Diborylmethane

机译：烯烃型氨基甲酰氯和1,1-二苯甲酸甲烷的Pd / Cu催化的Domino环化/扩张剂

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摘要

Reported herein is a palladium/copper cooperative-catalyzed dicarbofunctionalization of alkene-tethered carbamoyl chlorides with 1,1-diborylmethane. This cyclization/deborylation cascade strategy allows for the expedient formation of the versatile borylated 3,3-disubstituted oxindole skeleton, allowing for further functionalization via the derivatization of the carbon-boron bond.

机译：本文报道的是钯/铜协同催化的烯烃催化的烯烃型氨基甲酰氯二官能化，其具有1,1-二硼甲烷。该环化/扩张性级联策略允许通过碳 - 硼键的衍生化允许进一步官能化的多功能促进的3,3-二取代的氧胆固氧吲哚骨架。

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来源
《Organic letters》 |2020年第16期|共6页
作者
Zhang Chenhuan; Wu Xianqing; Wang Chenchen; Zhang Chengxi; Qu Jingping; Chen Yifeng;
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作者单位

East China Univ Sci &

Technol Feringa Nobel Prize Scientist Joint Res Ctr Frontiers Sci Ctr Materiobiol &

Dynam Chem Sch Chem &

Mol Engn Key Lab Adv Mat Shanghai 200237 Peoples R China;

East China Univ Sci &

Technol Feringa Nobel Prize Scientist Joint Res Ctr Frontiers Sci Ctr Materiobiol &

Dynam Chem Sch Chem &

Mol Engn Key Lab Adv Mat Shanghai 200237 Peoples R China;

East China Univ Sci &

Technol Feringa Nobel Prize Scientist Joint Res Ctr Frontiers Sci Ctr Materiobiol &

Dynam Chem Sch Chem &

Mol Engn Key Lab Adv Mat Shanghai 200237 Peoples R China;

East China Univ Sci &

Technol Feringa Nobel Prize Scientist Joint Res Ctr Frontiers Sci Ctr Materiobiol &

Dynam Chem Sch Chem &

Mol Engn Key Lab Adv Mat Shanghai 200237 Peoples R China;

East China Univ Sci &

Technol Feringa Nobel Prize Scientist Joint Res Ctr Frontiers Sci Ctr Materiobiol &

Dynam Chem Sch Chem &

Mol Engn Key Lab Adv Mat Shanghai 200237 Peoples R China;

East China Univ Sci &

Technol Feringa Nobel Prize Scientist Joint Res Ctr Frontiers Sci Ctr Materiobiol &

Dynam Chem Sch Chem &

Mol Engn Key Lab Adv Mat Shanghai 200237 Peoples R China;

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正文语种 eng
中图分类有机化学;
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1. Pd/Cu-Catalyzed Domino Cyclization/Deborylation of Alkene-Tethered Carbamoyl Chloride and 1,1-Diborylmethane [J] . Zhang Chenhuan, Wu Xianqing, Wang Chenchen, Organic letters . 2020,第16期

机译：烯烃型氨基甲酰氯和1,1-二苯甲酸甲烷的Pd / Cu催化的Domino环化/扩张剂
2. Synthesis of substituted γ-lactam via Pd(0)-catalyzed cyclization of alkene-tethered carbamoyl chloride [J] . Chen Chen, Jian Hu, Jianhua Su Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第21期

机译：通过Pd（0）催化的链烯键连接的氨基甲酰氯的环化反应合成取代的γ-内酰胺
3. Synthesis of substituted γ-lactam via Pd(0)-catalyzed cyclization of alkene-tethered carbamoyl chloride [J] . Chen Chen, Jian Hu, Jianhua Su Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第21期

机译：通过Pd（0）催化的链烯键连接的氨基甲酰氯的环化反应合成取代的γ-内酰胺
4. Study on the Cyclization of R-(+)-1,1' -Bi-2-Naphthol with o-phthalyl Chloride [C] . Jing Li, Zhuobin Shang, Shuo Jin, 11th International Symposium of Fine Chemistry and Functional Polymers Jul 28-31, 2001 Hailar, Inner Mongolia, P.R. China . 2001

机译：R-（+）-1,1'-Bi-2-萘酚与邻苯二甲酰氯环化的研究
5. Synthesis of Indolines via a Domino Cu-Catalyzed Amidation/Cyclization Reaction [O] . Ana Minatti, Stephen L. Buchwald -1

机译：通过多米诺铜催化的酰胺化/环化反应合成二氢吲哚
6. Pd/Cu-Catalyzed Domino Cyclization/Deborylation of Alkene-Tethered Carbamoyl Chloride and 1,1-Diborylmethane [O] . -1

机译：烯烃型氨基甲酰氯和1,1-二苯甲酸甲烷的Pd / Cu催化的Domino环化/扩张剂
7. Separation of HI-6 (4-Carbamoyl-2'-Hydroxyiminomethyl-1,1'-Oxydimethylen-Di(Pyridinium Chloride)) and Its Degradation Products by Ion-Pair High-Performance Liquid Chromatography [R] . Brown, N. D., Stermer-Cox, M. G., Doctor, B. P., 1984

机译：离子对高效液相色谱法分离HI-6（4-氨基甲酰-2'-羟基亚氨基甲基-1,1'-氧二亚甲基二（吡啶鎓氯化物））及其降解产物

Pd/Cu-Catalyzed Domino Cyclization/Deborylation of Alkene-Tethered Carbamoyl Chloride and 1,1-Diborylmethane

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