Synthesis, structure and properties of nickel and copper complexes containing <ce:italic>N,O</ce:italic>-hydrazone Schiff base ligand

María del Mar Conejo; Jorge Cantero; Antonio Pastor; Eleuterio álvarez; Agustín Galindo

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Synthesis, structure and properties of nickel and copper complexes containing N,O-hydrazone Schiff base ligand

机译：含有 n，o -ofdrozone schiff碱配体的合成，结构和性质

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Graphical abstract

Complexes [M(LNNMePh)2] (M=Ni,1; Cu,2) were synthesized and characterized. These compounds are the first structurally characterized transition metal complexes containing the κ2-N,O-2-(1-(2-methyl-2-phenylhydrazono)ethyl)phenolate ligand, LNNMePh.

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Highlights

?The compound HLNNMePhare prepared by a solvent-free synthetic procedure.

?Complexes [M(LNNMePh)2] (M=Ni,1; Cu,2) are synthesized and characterized.

?The first structurally characterized complexes with the LNNMePhligand are reported.

机译：<！[cdata [

图形摘要

复合物[M（l nnmeph ） 2 ]（m = ni， 1 ; cu， 2 ）被合成并表征。这些化合物是含有κ 2> sup> - n ， o的第一个结构表征金属复合物 -2-（1-（2-甲基-2-苯基羟基芳基）乙基）酚酸乙酯配体，L nnmeph 。否则省略

突出显示

？化合物HL Nnmeph 由无溶剂的合成程序制备。

？复合物[M（l nnmeph ） 2 ]（m = ni， 1 ; CU， 2 ）是合成的，其特征。

第一个结构表征与l nnmeph 配体是报道。

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来源
《Inorganica Chimica Acta》 |2018年第2018期|共6页
作者
María del Mar Conejo; Jorge Cantero; Antonio Pastor; Eleuterio álvarez; Agustín Galindo;
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作者单位

Departamento de Química Inorgánica Facultad de Química Universidad de Sevilla;

Departamento de Química Inorgánica Facultad de Química Universidad de Sevilla;

Departamento de Química Inorgánica Facultad de Química Universidad de Sevilla;

Instituto de Investigaciones Químicas CSIC–Universidad de Sevilla;

Departamento de Química Inorgánica Facultad de Química Universidad de Sevilla;

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原文格式 PDF
正文语种 eng
中图分类无机化学;
关键词
Copper; Nickel; Oxidation; Catalysis; Schiff base; DFT;

机译：铜;镍;氧化;催化;Schiff Base;DFT;

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专利

1. Synthesis, structure and properties of nickel and copper complexes containing N,O-hydrazone Schiff base ligand [J] . María del Mar Conejo, Jorge Cantero, Antonio Pastor, Inorganica Chimica Acta . 2018,第期

机译：含有 n，o -ofdrozone schiff碱配体的合成，结构和性质
2. ONO donor hydrazone ligand: Synthesis, characterization, crystallographic insight, in?vivo and in?vitro anti-inflammatory activity]]> [J] . Umashri Kendur, Geeta H. Chimmalagi, Sunil M. Patil, Journal of Molecular Structure . 2018,第期

机译：<！[CDATA [CDATA [CDATAL后期第一行过渡金属复合物 ONO 供体腙配体：合成，表征，晶体洞察力， In？Vivo 和在？体外抗炎活动]]]>
3. Syntheses, structures, and inhibition studies of Jack bean urease by copper(II) complexes derived from a tridentate hydrazone ligand [J] . Zhonglu You, Huiyuan Yu, Boyang Zheng, Inorganica Chimica Acta . 2018,第期

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4. Synthesis, Characterization and Ligand Field Parametrization in Complex Compounds of Nickel(Ⅱ) and Copper(Ⅱ) with Hydrazone Schiff Bases [C] . Mirela Calinescu, Emilia Ion, Ana Emandi, . 2001

机译：Hy席夫碱镍（Ⅱ）和铜（Ⅱ）配合物的合成，表征及配体场参数化
5. Asymmetric synthesis of stereochemically-defined and conformationally-constrained novel amino acids via direct alkylation of chiral nickel(II)-coordinated Schiff bases of glycine and alanine, and design and synthesis of selective peptide and non-peptide ligands for the delta-opioid receptor. [D] . Tang, Xue-jun. 2002

机译：通过手性镍（II）配位的甘氨酸和丙氨酸的席夫碱直接烷基化的立体化学定义和构象约束的新型氨基酸的不对称合成，以及δ阿片受体的选择性肽和非肽配体的设计和合成。
6. Synthesis of Two Potentially Heptadentate (N4O3) Schiff-base Ligands Derived from Condensation of Tris(3-aminopropyl)-amine and Salicylaldehyde or 4-Hydroxysalicylaldehyde. Nickel(II) and Copper(II) Complexes of the Former Ligand. [O] . Hassan Keypour, Sadegh Salehzadeh, R. V. Parish 2002

机译：三（3-氨基丙基）-胺与水杨醛或4-羟基水杨醛缩合衍生的两种潜在的七齿（N4O3）Schiff碱配体的合成。前配体的镍（II）和铜（II）配合物。
7. Synthesis of Two Potentially Heptadentate (N4O3) Schiff-base Ligands Derived from Condensation of Tris(3-aminopropyl)-amine and Salicylaldehyde or 4-Hydroxysalicylaldehyde. Nickel(II) and Copper(II) Complexes of the Former Ligand [O] . R. V. Parish, Sadegh Salehzadeh, Hassan Keypour 2002

机译：三（3-氨基丙基）胺与水杨醛缩丁醛或4-羟基水杨醛缩合生成的两种潜在的三齿（N4O3）席夫碱配体的合成。前配体的镍（II）和铜（II）配合物
8. Research on the Influence of the Nature of the Ligand on the Stereochemistry Try of the Nickel (II) and Other 1st Row Transition Metal Complexes with Schiff Bases [R] . Sacconi, L. 1964

机译：配体性质对镍（Ⅱ）和其他第一行schiff碱过渡金属配合物立体化学试验的影响

Synthesis, structure and properties of nickel and copper complexes containing N,O-hydrazone Schiff base ligand

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