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Gum arabic capped copper nanoparticles: Synthesis, characterization, and applications

机译:胶阿拉伯盖铜纳米粒子:合成,表征和应用

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In present work, we synthesized copper nanoparticles using l-ascorbic acid as a reducing agent and capped them with gum arabic. Based upon spectrometric analysis and particle size distribution (19.60-35.06 nm) by intensity, a 1% concentration of gum arabic was selected as the suitable capping agent for copper nanoparticles. Gum arabic capped copper nanoparticles revealed significantly (p < 0.05) higher zeta potential value than that of unmodified copper nanoparticles. Energy-dispersive X-ray spectroscopy revealed the purity of the copper nanoparticles, whereas scanning electron microscopy confirmed the polygonal prismatic shape of the gum arabic capped copper nanoparticles. As well, TEM analysis confirmed the monodispersed nature of the gum arabic capped copper nanoparticles. Gum arabic capped copper nanoparticles showed significantly (p < 0.05) higher zone of inhibition for Salmonella typhimurium (27 mm) than that of other bacterial strains. Approximately 95% photocatalytic degradation of methylene blue and crystal violet was observed within 40 and 20 min. As well, both unmodified and gum arabic capped copper nanoparticles were found to be non-toxic to Caco-2 cells during cell viability assay. (C) 2020 Elsevier B.V. All rights reserved.
机译:在目前的工作中,我们使用L-抗坏血酸作为还原剂合成铜纳米颗粒,并用阿拉伯树胶封装它们。基于光谱分析和粒度分布(19.60-35.06nm)强度,选择1%的胶阿拉伯植物作为铜纳米颗粒的合适的封端剂。胶阿拉伯盖铜纳米颗粒显着显着(P <0.05)均高于未改性铜纳米颗粒的Zeta电位值。能量分散X射线光谱显示铜纳米颗粒的纯度,而扫描电子显微镜证实了胶阿拉伯盖铜纳米粒子的多边形棱柱形状。同样,TEM分析证实了牙龈阿拉伯胶铜纳米粒子的单分裂性质。胶阿拉伯盖铜纳米粒子显着(P <0.05)抑制沙门氏菌(27mm)比其他细菌菌株更高的抑制区。在40和20分钟内观察到约95%的光催化降解亚甲基蓝色和晶体紫。同样,在细胞活力测定期间发现未修饰的阿拉伯盖铜纳米粒子对Caco-2细胞无毒。 (c)2020 Elsevier B.v.保留所有权利。

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