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Synthesis of Silver Nanoparticles of Corn Silk Agrowaste and Their Bioactivities

机译:玉米丝绸纳米粒子的合成及其生物活跃

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Present study was intended to synthesize silver nanoparticles (AgNPs) using corn silk aqueous extract (CSAE) and evaluate for antimicrobial and antiurolithiatic potential. The aqueous decoction of corn silk offered light yellow CSAE. Treatment of AgNO3 with CSAE offered AgNPs with absorbance 430 nm. Optimization study established 5 mM silver nitrate, 2.5:7.5 extract to AgNO3 ratio, pH 8, and 24 h time as parametric requirement for synthesis of AgNPs using CSAE. Stability study supported the AgNPs stability based on retention of SPR signal between 428 to 450 nm. The synthesis of AgNPs was confirmed on broad and shifted FTIR bands; XRD signals at 20 values of 32.27°, 40.72°, 46.20°, 65.69°, 69.31° and 76.49° indexed to 111, 200, 220 and 311 planes, respectively; particle size range from 22.05-36.69 nm in FESEM; and elemental silver content of 62.17% as per EDX spectrum. The synthesized AgNPs exhibited high antibacterial and antiurolithiatic potential. Present study recommends that synthesis of AgNPs using CSAE is a facile and eco-friendly method.
机译:目前的研究旨在使用玉米丝含水提取物(CSAE)合成银纳米颗粒(AgNP),评价抗微生物和抗腐蚀剂潜力。玉米丝的水性汤剂提供浅黄色CSAE。用CSAE治疗AgNO3提供吸光度430nm的AgNP。优化研究建立了5毫米硝酸银,2.5:7.5提取至AgNO3比例,pH8和24小时,作为使用CSAE合成AgNP的参数要求。稳定性研究支持基于428至450nm之间的SPR信号的保留率稳定性。在宽和移位的FTIR带上确认了AgNP的合成; XRD信号以20值为32.27°,40.72°,46.20°,65.69°,69.31°和76.49°分别分别指定为111,200,220和311平面;粒度范围为22.05-36.69 nm在FeSEM中;根据EDX光谱,元素银含量为62.17%。合成的agnps表现出高抗菌和抗腐蚀剂潜力。本研究建议使用CSAE合成AgNP是一种容易和环保的方法。

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