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Fabrication and characterization of Ni-Zr composite coatings using electrodepositing technique

机译:电沉积技术制备Ni-Zr复合镀层及其表征

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The main goal of this research is to prepare Ni-Zr composite coatings with different amounts of Zr microparticles by using electrodeposition technology. Different characterization techniques including X-ray diffractometer (XRD), field emission scanning electron microscopy (FESEM) and Energy Dispersive Xray Spectroscopy (EDX) were used to investigate the effects of Zr micro-particle contents on the surface morphology, texture, grain size, residual stress and hardness of the Ni-Zr composite coatings. The electrochemical impedance and potentiodynamic polarization measurements were also used to examine the corrosion resistance. As the Zr contents in the Ni-Zr composite coating increased, the (200) texture changed to the (111) texture, the grain size decreased, the residual stress and hardness increased. The anti-corrosion properties of the Ni-Zr composite coatings could be linked to several reasons such as the amount of Zr micro-particles in the deposits, a decrease in grain size, and a change in the texture of the deposits. (C) 2015 Elsevier B.V. All rights reserved.
机译:本研究的主要目的是通过电沉积技术制备具有不同数量Zr微粒的Ni-Zr复合涂层。 X射线衍射仪(XRD),场发射扫描电子显微镜(FESEM)和能量色散X射线光谱仪(EDX)等不同的表征技术用于研究Zr微粒含量对表面形态,织构,晶粒尺寸, Ni-Zr复合涂层的残余应力和硬度。电化学阻抗和电位动力学极化测量结果也用于检查耐腐蚀性。随着Ni-Zr复合涂层中Zr含量的增加,(200)织构变为(111)织构,晶粒尺寸减小,残余应力和硬度增加。 Ni-Zr复合涂层的抗腐蚀性能可能与多种原因有关,例如沉积物中Zr微粒的数量,晶粒尺寸的减小以及沉积物质地的变化。 (C)2015 Elsevier B.V.保留所有权利。

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