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Synthesis of polyaniline nanoparticle grafted silica gel and study of its Cr(VI) binding property

机译:聚苯胺纳米粒子接枝硅胶的合成及其对Cr(VI)结合性能的研究

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Polyaniline nanoparticles have been synthesized through simple micelle technique and then grafted it with silanized silica gel to develop a novel hybrid material. The nanoparticles are characterized by UV-Vis, TEM, CV, SEM, TGA, DTG, and DSC. Silanization and grafting reactions are evaluated by FTIR and chemical test. The Cr(VI) binding behavior of the composite is studied in various pH of the medium, and both competitive and noncompetitive conditions. The particle size, adsorption capacity, and surface area of the material are found to be 100 nm, 135 mg/g, and 720 m~2/g, respectively.
机译:通过简单的胶束技术合成了聚苯胺纳米颗粒,然后将其与硅烷化硅胶接枝以开发新型杂化材料。纳米颗粒的特征在于紫外可见光,透射电镜,CV,SEM,TGA,DTG和DSC。通过FTIR和化学测试评估硅烷化和接枝反应。在介质的各种pH值以及竞争性和非竞争性条件下研究了复合材料的Cr(VI)结合行为。发现该材料的粒径,吸附容量和表面积分别为100nm,135mg / g和720m 2 / g。

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