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New polyphenol derivative in Ipomoea batatas tubers and its antioxidant activity

机译:番薯块茎中的新型多酚衍生物及其抗氧化活性

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Four different polyphenolic compounds were isolated by chromatographic methods from methanolic and hydromethanolic extracts of Ipomoea batatas tuber flour. On the basis of UV, mass, and NMR analysis procedures, the structure of the isolated compounds were determined as 4,5-di-O-caffeoyldaucic acid (1), 4-O-caffeoylquinic acid (2), 3,5-di-O-caffeoylquinic acid (3), and 1,3-di-O-caffeoylquinic acid (4). To the best of our knowledge, this is the first report of isolation and characterization of compound 1. Then, we evaluated the antioxidant activity of daucic acid derivative by using DPPH and FRAP methods together with authentic antioxidant standards, L-ascorbic acid, tert-butyl-4-hydroxy toluene (BHT), and gallic acid. The activity of compound 1 in both methods was higher than that of all standards used at the same molar concentration.
机译:通过色谱法从番薯块茎粉的甲醇和氢甲醇提取物中分离出四种不同的多酚化合物。根据UV,质量和NMR分析程序,确定了分离出的化合物的结构,分别为4,5-二-O-咖啡酰甜菜碱酸(1),4-O-咖啡酰奎宁酸(2),3,5-二-O-咖啡酰奎尼酸(3)和1,3-二-O-咖啡酰奎尼酸(4)。据我们所知,这是化合物1的分离和表征的第一份报告。然后,我们通过使用DPPH和FRAP方法以及正宗的抗氧化剂标准品L-抗坏血酸,叔丁基丁基-4-羟基甲苯(BHT)和没食子酸。两种方法中化合物1的活性均高于相同摩尔浓度下使用的所有标准品的活性。

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