A metal-free addition/dearomatization-cyclization/decarboxylation cascade of aryl 3-arylpropiolate toward the synthesis of 1,1-diaryl-2-alkyl-substituted ethylenes

Wang Jie; Mou Xue-Qing; Zhang Bang-Hong; Liu Wei-Ting; Yang Chao; Xu Li; Xu Zheng-Liang; Wang Shao-Hua

首页> 外文期刊>Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry >A metal-free addition/dearomatization-cyclization/decarboxylation cascade of aryl 3-arylpropiolate toward the synthesis of 1,1-diaryl-2-alkyl-substituted ethylenes

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A metal-free addition/dearomatization-cyclization/decarboxylation cascade of aryl 3-arylpropiolate toward the synthesis of 1,1-diaryl-2-alkyl-substituted ethylenes

机译：3-金属芳基丙酸酯的无金属加成/脱芳构环-脱羧级联反应，合成1,1-二芳基-2-烷基取代的乙烯

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摘要

A radical-participated addition/dearomatization-cyclization/decarboxylation cascade between aryl 3-arylpropiolate and ethers (cycloalkane) has been developed to give a series of 1,1,2-trisubstituted ethylenes in moderate to good yields. (C) 2016 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2016年第11期|共4页
作者
Wang Jie; Mou Xue-Qing; Zhang Bang-Hong; Liu Wei-Ting; Yang Chao; Xu Li; Xu Zheng-Liang; Wang Shao-Hua;
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正文语种 eng
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Tandem reaction; 1; 1; 2-Trisubstituted ethylenes; Aryl 3-arylpropiolate; Decarboxylation;

机译：串联反应;1;1;2-三取代的乙烯;3-芳基丙酸芳酯;脱羧;

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1. A metal-free addition/dearomatization-cyclization/decarboxylation cascade of aryl 3-arylpropiolate toward the synthesis of 1,1-diaryl-2-alkyl-substituted ethylenes [J] . Wang Jie, Mou Xue-Qing, Zhang Bang-Hong, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2016,第11期

机译：3-金属芳基丙酸酯的无金属加成/脱芳构环-脱羧级联反应，合成1,1-二芳基-2-烷基取代的乙烯
2. Oxidative difunctionalization of alkynoates via cascade radical addition, aryl migration, and decarboxylation [J] . Pan Changduo, Zhang Honglin, Zhu Chengjian Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2016,第5期

机译：通过级联自由基加成，芳基迁移和脱羧作用，炔酸的氧化双官能化
3. A facile synthesis of isoindoline and Δ~1 -pyrrolines from chalcone and glycine by a cascade of process involving addition, in situ decarboxylation, and cyclization [J] . Elangovan Elamparuthi, Subramaniayan Sarathkumar, Swaminathan Girija Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2014,第29期

机译：通过查尔酮和甘氨酸通过包括加成，原位脱羧和环化在内的一系列步骤轻松合成异吲哚啉和Δ〜1-吡咯啉
4. Synthesis and Reactions of Dinuclear Alkyl-,Aryl- and Allylplatinum-PIatinum (or -Palladium) Complexes by Oxidative Addition to Platinum(O) Complex [C] . Nobuyuki Komine, Tomoko Ishiwata, Jun-ya Kasahara, Symposium on Organometallic Chemistry . 2004

机译：通过氧化添加到铂（O）复合物的氧化添加剂（O）复合物的二核烷基 - ，芳基和烯丙基 - 吡啶 - 吡啶（或-Palladium）配合物的合成与反应
5. Part I. Asymmetric hydrosilylation of acetophenone using titanium catalysts. Part II. Synthesis of water-soluble palladacycles and their applications to the Suzuki reaction. Part III. Rhodium-catalyzed addition of aryl and alkenylboronic acids to aldehyde [D] . Huang, Rongcai. 2005

机译：第一部分：使用钛催化剂的苯乙酮不对称氢化硅烷化。第二部分水溶性palladacycles的合成及其在铃木反应中的应用。第三部分铑催化的芳基和烯基硼酸加成醛
6. Homologation of α-Aryl Amino Acids through Quinone-Catalyzed Decarboxylation/Mukaiyama–Mannich Addition [O] . Benjamin J. Haugeberg, Johnny H. Phan, Xinyun Liu, -1

机译：通过醌催化的脱羧/ Mukaiyama–Mannich加成的α-芳基氨基酸的同系化
7. Inside Back Cover: A Fluorination/Aryl Migration/Cyclization Cascade for the Metal-Free Synthesis of Fluoro-Benzoxazepines (Chem. Eur. J. 11/2016) [O] . Anna Ulmer, Christoph Brunner, Andreas M. Arnold, 2016

机译：内盖：氟化/芳基迁移/环化级联，用于无金属合成氟 - 苯并恶化（Chem.Eur。J.11/2016）

A metal-free addition/dearomatization-cyclization/decarboxylation cascade of aryl 3-arylpropiolate toward the synthesis of 1,1-diaryl-2-alkyl-substituted ethylenes

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