A one-pot, catalyst-free synthesis of novel 2-thioxo-tetrahydropyrimidine derivatives via the three-component reaction of alkyl chloroglyoxalates, alkyl isocyanides, and thioureas

Moradi Loghman; Bahrami Chonor; Mirzaei Anvar; Zarehbin Mohammad Rezgar; Yavari Issa

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A one-pot, catalyst-free synthesis of novel 2-thioxo-tetrahydropyrimidine derivatives via the three-component reaction of alkyl chloroglyoxalates, alkyl isocyanides, and thioureas

机译：通过烷基氯乙二酸酯，烷基异氰化物和硫脲的三组分反应，一锅无催化剂地合成新型2-硫代-四氢嘧啶衍生物

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alpha-Ketoimidoyl chlorides, obtained from the alpha-addition of acyl chlorides to alkyl isocyanides are treated with thiourea derivatives to afford novel 2-thioxo-tetrahydropyrimidine derivatives in good to excellent yields. (C) 2015 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2015年第12期|共3页
作者
Moradi Loghman; Bahrami Chonor; Mirzaei Anvar; Zarehbin Mohammad Rezgar; Yavari Issa;
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正文语种 eng
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alpha-Ketoimidoyl chlorides; Alkyl isocyanides; 2-Thioxo-tetrahydropyrimidines; Thiourea; Acyl chlorides;

机译：α-酮亚氨基酰氯;烷基异氰化物;2-硫代-四氢嘧啶;硫脲;酰氯;

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1. A one-pot, catalyst-free synthesis of novel 2-thioxo-tetrahydropyrimidine derivatives via the three-component reaction of alkyl chloroglyoxalates, alkyl isocyanides, and thioureas [J] . Moradi Loghman, Bahrami Chonor, Mirzaei Anvar, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015,第12期

机译：通过烷基氯乙二酸酯，烷基异氰化物和硫脲的三组分反应，一锅无催化剂地合成新型2-硫代-四氢嘧啶衍生物
2. A Novel Three-Component Reaction of Dibenzylamine and an Aromatic Aldehyde with an Alkyl Isocyanide in the Presence of Silica Gel: An Efficient Route for the One-Pot Synthesis of Sterically Congested 2-(Dibenzylamino)-2-Aryl Acetamide Derivatives [J] . Ahmadi E, Mahyari AT, Ramazani A, Letters in organic chemistry . 2008,第7期

机译：在硅胶存在下二苄基胺和芳香醛与烷基异氰酸酯的新型三组分反应：单罐合成立体拥挤的2-（二苄基氨基）-2-芳基乙酰胺衍生物的有效途径
3. One-pot, three-component condensation of 2-hydroxybenzaldehyde derivatives, primary amines with alkyl isocyanides to N-alkyl-2-(2-hydroxyphenyl)-2-imino-acetamides [J] . Mehdi Ghandi, Parham Asgari, Abuzar Taheri Central European Journal of Chemistry . 2010,第4期

机译：一锅，三组分的2-羟基苯甲醛衍生物，伯胺与烷基异氰化物的缩合反应，生成N-烷基-2-（2-羟基苯基）-2-亚氨基乙酰胺
4. Ionic Liquid-Accelerated Three-Component Reaction——A Rapid One-Pot Synthesis of 3-substituted-5-arylidene-4-thi-azolidinone Derivatives [C] . 7th International Symposium on Green Chemistry in China(7th ISGCC'2005) . 2005

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5. One-pot approach to various 2-alkyl/arylbenzothiazinones and 2-alkyl/arylbenzothiazoles using microwave-assisted organic systems. [D] . Koh, Benjamin. 2007

机译：使用微波辅助有机系统，一锅法制备各种2-烷基/芳基苯并噻嗪酮和2-烷基/芳基苯并噻唑。
6. A Novel Synthesis of Highly Functionalized Pyridines by a One-Pot Three-Component Tandem Reaction of Aldehydes Malononitrile and N-Alkyl-2-cyanoacetamides under Microwave Irradiation [O] . Ramadan Ahmed Mekheimer, Mariam Abdullah Al-Sheikh, Hanadi Yousef Medrasi, 2018

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7. One-pot, three component reactions between isocyanides and dialkyl acetylenedicarboxylates in the presence of phenyl isocyanate: synthesis of dialkyl 2-(alkyl/arylimino)-2,5-dihydro-5-oxo-1-phenyl-1H-pyrrole-3,4-dicarboxylate [O] . Khatereh Khandan-Barani, Malek T. Maghsoodlou, Nourallah Hazeri, 2011

机译：在异氰酸苯酯存在下异氰化物与乙炔二羧酸二烷基酯之间的一锅三组分反应：2-（烷基/芳基亚氨基）-2,5-二氢-5-氧代-1-苯基-1H-吡咯-3-二烷基酯的合成， 4二羧酸酯

A one-pot, catalyst-free synthesis of novel 2-thioxo-tetrahydropyrimidine derivatives via the three-component reaction of alkyl chloroglyoxalates, alkyl isocyanides, and thioureas

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