Facile and efficient synthesis of hydroxyalkyl esters from cyclic acetals through aerobic photo-oxidation using anthraquinone-2-carboxylic acid

Yamaguchi Tomoaki; Kudo Yasuhisa; Hirashima Shin-ichi; Yamaguchi Eiji; Tada Norihiro; Miura Tsuyoshi; Itoh Akichika

首页> 外文期刊>Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry >Facile and efficient synthesis of hydroxyalkyl esters from cyclic acetals through aerobic photo-oxidation using anthraquinone-2-carboxylic acid

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Facile and efficient synthesis of hydroxyalkyl esters from cyclic acetals through aerobic photo-oxidation using anthraquinone-2-carboxylic acid

机译：使用蒽醌-2-羧酸通过需氧光氧化从环缩醛中快速有效地合成羟烷基酯

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摘要

A convenient metal-free oxidation protocol of various cyclic acetals with molecular oxygen and anthraquinone-2-carboxylic acid under visible light irradiation by a fluorescent lamp afforded their corresponding hydroxyalkyl esters. (C) 2015 Elsevier Ltd. All rights reserved.

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2015年第15期|共3页
作者
Yamaguchi Tomoaki; Kudo Yasuhisa; Hirashima Shin-ichi; Yamaguchi Eiji; Tada Norihiro; Miura Tsuyoshi; Itoh Akichika;
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正文语种 eng
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关键词
Aerobic; Oxidation; Visible light; Anthraquinone;

机译：有氧;氧化;可见光;蒽醌;

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1. Facile and efficient synthesis of hydroxyalkyl esters from cyclic acetals through aerobic photo-oxidation using anthraquinone-2-carboxylic acid [J] . Yamaguchi Tomoaki, Kudo Yasuhisa, Hirashima Shin-ichi, Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2015,第15期

机译：使用蒽醌-2-羧酸通过需氧光氧化从环缩醛中快速有效地合成羟烷基酯
2. Sulfamic acid-mediated, efficient, one-pot synthesis of novel 5-substituted 1,3,4-thiadiazol-2-ylcarbamoyl aliphatic amide acid derivatives and facile synthesis of cyclic amides [J] . Toche R.B., Janrao R.A., Gangurde S.A., Synthetic Communications . 2013,第16a18期

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3. Preparation of Resin-Bound Bismethylene Cyclic Malonic Acid Ester and Facile Solid-Phase Synthesis of 2-Alkylthio-4(1H)-quinolone synthesis of 2-Alkyl-4(1H)-quinolone [J] . Jing Tang, Xian Huang Synthetic Communications . 2003,第22期

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4. Water Determines the Selectivity: Facile Room Temperature C-O Cleavage of P(III) Esters by Br?nsted Acids Leading to a Mild and Efficient Halide-Free Michaelis–Arbuzov Rearrangement [C] . Chunya Li, Jianqiu Zhang, Jingjing Ye 日本化学会春季年会講演予稿集 . 2018

机译：水决定了选择性：Br的选择性：Br的P（III）酯的C-O裂解乳酸的乳酸，导致无温和和高效的卤化物Michaelis-Arbuzov重排
5. Tandem aza[4+2]/allylboration: A novel multicomponent reaction for the stereocontrolled synthesis of α-hydroxyalkyl piperidine derivatives, and, N,N-diethanolaminomethyl polystyrene: An efficient solid support to immobilize boronic acids [D] . Tailor, Jyotiben M. 2000

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6. Cyclic Acetal Formation Between 2-Pyridinecarboxaldehyde and γ-Hydroxy-αβ-Acetylenic Esters [O] . Sami Osman, Kazunori Koide -1

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7. Nitroketene Acetal Chemistry. 3. Facile Synthesis of Nitroacetic Acid Triarylmethyl Ortho Esters from 1, 1-Di(methylsulfanyl)-2-nitroethylene [O] . -1

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Facile and efficient synthesis of hydroxyalkyl esters from cyclic acetals through aerobic photo-oxidation using anthraquinone-2-carboxylic acid

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