Synthesis of β-carbolines using microwave-assisted aza-Wittig methodology in ionic liquids

Pilar M. Fresneda; Jose Antonio Blazquez

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Synthesis of β-carbolines using microwave-assisted aza-Wittig methodology in ionic liquids

机译：微波辅助氮杂-维蒂希方法在离子液体中合成β-咔啉

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The improved preparation of 1-substituted-β-carbolines is reported using microwave-assisted aza-Wittig/electrocyclic ring-closure reaction with ionic liquids as solvent. In all cases an unprecedented N-methoxymethyl group (MOM) deprotection is observed.

机译：据报道，使用微波辅助的以离子液体为溶剂的氮杂-维蒂希/电环闭合反应，改进了1-取代-β-咔啉的制备方法。在所有情况下，均观察到前所未有的N-甲氧基甲基（MOM）脱保护。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2012年第21期|共4页
作者
Pilar M. Fresneda; Jose Antonio Blazquez;
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正文语种 eng
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关键词
β-Carbolines; Iminophosphoranes; Aza-Wittig reaction; Microwave irradiation; Ionic liquids;

机译：β-咔啉;亚氨基正膦;氮杂-维蒂希反应;微波辐射;离子液体;

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专利

1. Synthesis of β-carbolines using microwave-assisted aza-Wittig methodology in ionic liquids [J] . Pilar M. Fresneda, Jose Antonio Blazquez Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2012,第21期

机译：微波辅助氮杂-维蒂希方法在离子液体中合成β-咔啉
2. Heterogeneous microwave-assisted Ullmann type methodology for synthesis of rigid-core ionic liquid crystals [J] . Fouchet Julien, Heinrich Benoit, LHer Matthieu, New Journal of Chemistry . 2018,第12期

机译：非均相微波辅助ULLmann型方法，用于合成刚性核离子液晶晶体
3. Optimised microwave-assisted synthesis of methylcarbonate salts: a convenient methodology to prepare intermediates for ionic liquid libraries [J] . John D. Holbrey, Robin D. Rogers, Saloni S. Shukla Green chemistry . 2010,第3期

机译：优化的微波辅助合成碳酸甲酯盐：制备离子液体库中间体的简便方法
4. Study on microwave-assisted synthesis of ionic liquids based on dialkylimidazolium [C] . Hu Zhu, Youming Li, Xiaofang Wan International conference on biotechnology, chemical and materials engineering . 2012

机译：二烷基咪唑基微波辅助合成离子液体的研究
5. Synthesis of Ionic Liquids and Magnetic Ionic Liquids and Their Application in Dispersive Liquid-liquid Microextraction [D] . Pierson, Stephen A. 2018

机译：离子液体和磁性离子液体的合成及其在分散液-液微萃取中的应用
6. Microwave-Assisted Synthesis of Some Potential Bioactive Imidazolium-Based Room-Temperature Ionic Liquids [O] . Ahmed H. Albalawi, Wael S. El-Sayed, Ateyatallah Aljuhani, 2018

机译：微波辅助合成的一些潜在的基于生物活性咪唑的室温离子液体
7. Reaction of o-Aminobenzamides with Dialkyl Carbonates and Ionic Liquids: A Novel one-pot, High-yield, Microwave-assisted Synthesis of 1-Alkylquinazoline-2,4-diones [O] . Leticia Guerrero R., Ignacio A. Rivero 2017

机译：O-氨基苯甲酰胺与碳酸二烷基酯和离子液体的反应：一种新的单罐，高收率，微波辅助合成1-烷基喹唑啉-2,4-致力

Synthesis of β-carbolines using microwave-assisted aza-Wittig methodology in ionic liquids

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