Microwave-assisted N-Boc deprotection under mild basic conditions using K3PO4·H2O in MeOH

Srinivasa Reddy Dandepally; Alfred L Williams

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Microwave-assisted N-Boc deprotection under mild basic conditions using K3PO4·H2O in MeOH

机译：在温和的碱性条件下，使用MeOH中的K3PO4·H2O进行微波辅助的N-Boc脱保护

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A simple and efficient method for the deprotection of secondary Boc-protected amino compounds under mild basic conditions using K3PO4·H2O in MeOH assisted by microwave irradiation has been presented.

机译：提出了一种简单有效的方法，在温和的碱性条件下，采用K3PO4·H2O在MeOH中的微波辐射辅助脱保护Boc保护的仲氨基化合物。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2009年第9期|共4页
作者
Srinivasa Reddy Dandepally; Alfred L Williams;
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1. Microwave-assisted N-Boc deprotection under mild basic conditions using K3PO4·H2O in MeOH [J] . Srinivasa Reddy Dandepally, Alfred L Williams Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2009,第9期

机译：在温和的碱性条件下，使用MeOH中的K3PO4·H2O进行微波辅助的N-Boc脱保护
2. Mild Deprotection of tert-Butyl Carbamates of NH-Heteroarenes under Basic Conditions [J] . Manas Chakrabarty, Taraknath Kundu, Yoshihiro Harigaya Synthetic Communications . 2006,第13a15期

机译：碱性条件下NH-杂芳烃氨基甲酸叔丁酯的轻度脱保护
3. Mild deprotection of tert-butyl carbamates of NH-heteroarenes under basic conditions [J] . Chakrabarty M, Kundu T, Harigaya Y Synthetic Communications . 2006,第14期

机译：在碱性条件下对NH-杂芳烃的氨基甲酸叔丁酯进行轻度脱保护
4. Microwave-Assisted FeCl_3·6H_2O-Catalyzed Regioselective Deprotection of Pyranose Anomeric O-Acetyl Group [C] . Qiang Wang, Guodong Liu, Shanshan Gong, International Conference on Material Engineering, Chemistry, Bioinformatics . 2014

机译：微波辅助FECL_3·6H_2O催化的吡喃糖异常O-乙酰基的区域选择性脱保护
5. I. Tertiary aryl sulfonamides as new cross coupling partners for nickel catalyzed Kumada-Corriu-Tamao reductive and carbon-carbon bond forming cross coupling reactions. II. N-sulfonyl deprotection under mild nickel(0) catalyzed Kumada-Corriu-Tamao coupling conditions and development of the N-Ans protecting group. III. Synthesis and application of 3,3'-di-(2-pyridyl)-1,1'-bi-2-naphthol ligands [D] . Milburn, Robert Ronald 2004

机译：I.叔芳基磺酰胺作为镍催化的Kumada-Corriu-Tamao还原和碳-碳键形成交叉偶联反应的新交叉偶联伴侣。二。在温和的镍（0）下N-磺酰基脱保护催化了Kumada-Corriu-Tamao偶联条件和N-Ans保护基的发展。三， 3,3'-二-（2-吡啶基）-1,1'-bi-2-萘酚配体的合成及应用
6. Efficient microwave-assisted solid phase coupling of nucleosides small library generation and mild conditions for release of nucleoside derivatives [O] . Hanumantharao Paritala, Yuta Suzuki, Kate S. Carroll -1

机译：核苷的高效微波辅助固相偶联小文库生成和核苷衍生物释放的温和条件
7. A Simple and Efficient Green Method for the Deprotection of N-Boc in Various Structurally Diverse Amines under Water-mediated Catalyst-free Conditions [O] . Aouf Nour-Eddine, Berredjem Malika, Jamel Zoubir, 2012

机译：一种简单高效的绿色方法，在无水介导的条件下，将各种结构多样的胺中的N-Boc脱保护

Microwave-assisted N-Boc deprotection under mild basic conditions using K3PO4·H2O in MeOH

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