Synthesis of stereodefined 1-aryl(heteroaryl) substituted 1,2-bis(2-bromopyridin-3-yl)ethenes by selective tandem Suzuki-Miyaura cross-coupling reactions

Giorgio Chelucci; Salvatore Baldino

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Synthesis of stereodefined 1-aryl(heteroaryl) substituted 1,2-bis(2-bromopyridin-3-yl)ethenes by selective tandem Suzuki-Miyaura cross-coupling reactions

机译：选择性串联铃木-宫浦交叉偶联反应合成立体定义的1-芳基（杂芳基）取代的1,2-双（2-溴吡啶-3-基）乙烯

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A protocol for the synthesis of stereodefined 1-aryl(heteroaryl) substituted 1,2-bis(2-bromopyridin-3-yl)ethenes by tandem Suzuki-Miyaura cross-coupling reactions and an example of convention into 5-phenyl-1,10-phenanthroline are described.

机译：Suzuki-Miyaura串联偶联反应合成立体定义的1-芳基（杂芳基）取代的1,2-双（2-溴吡啶基-3-基）乙烯的规程，以及将规例转化为5-苯基-1的例子，描述了10-菲咯啉。

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《Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry》 |2008年第17期|共5页
作者
Giorgio Chelucci; Salvatore Baldino;
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正文语种 eng
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关键词
Alkenes; Nitrogen heterocycles; Suzuki-Miyaura reaction; Palladium catalysts;

机译：烯烃;氮杂环;Suzuki-Miyaura反应;钯催化剂;

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1. Synthesis of stereodefined 1-aryl(heteroaryl) substituted 1,2-bis(2-bromopyridin-3-yl)ethenes by selective tandem Suzuki-Miyaura cross-coupling reactions [J] . Giorgio Chelucci, Salvatore Baldino Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 2008,第17期

机译：选择性串联铃木-宫浦交叉偶联反应合成立体定义的1-芳基（杂芳基）取代的1,2-双（2-溴吡啶-3-基）乙烯
2. One-pot dual substitutions of bromobenzyl chloride, 2-chloromethyl-6-halogenoimidazo[1,2-a]pyridine and -[1,2-b]pyridazine by Suzuki-Miyaura cross-coupling reactions [J] . Henry N, Enguehard-Gueiffier C, Thery I, European journal of organic chemistry . 2008,第28期

机译：Suzuki-Miyaura交叉偶联反应对溴苄氯，2-氯甲基-6-卤代咪唑并[1,2-a]吡啶和-[1,2-b]哒嗪进行一锅双取代
3. One-pot dual substitutions of bromobenzyl chloride, 2-chloromethyl-6-halogenoimidazo[1,2-a]pyridine and -[1,2-b]pyridazine by Suzuki-Miyaura cross-coupling reactions [J] . Henry N, Enguehard-Gueiffier C, Thery I, European journal of organic chemistry . 2008,第28期

机译：Suzuki-Miyaura交叉偶联反应对溴苄氯，2-氯甲基-6-卤代咪唑并[1,2-a]吡啶和-[1,2-b]哒嗪进行一锅双取代
4. Rationalizing the selectivity of the Suzuki-Miyaura cross-coupling reaction in the synthesis of 1-arylnaphthalenes and 1,8-diarylnaphthalenes. [C] . Carlos F. R. A. C. Lima, Luis M. N. B. F. Santos, Jose E. Rodriguez-Borges European Symposium on Organic Chemistry . 2009

机译：合理化Suzuki-Miyaura交叉偶联反应在合成1-芳基萘和1,8-二芳基萘中的选择性。
5. Functionalized organotrifluoroborates: Synthesis and reactivity. I.Suzuki-Miyaura reactions of aryl- and heteroaryl trifluoroborates with aryl- and heteroaryl triflates. II. Oxidation of hydroxyl-containing trifluoroborates. III. Suzuki-Miyaura reactions of potassium trifluoroboratohomoenolates. IV. Development of a HRMS method for organotrifluoroborates [D] . Petrillo, Daniel E. 2008

机译：功能化的有机三氟硼酸酯：合成与反应性。芳基-和杂芳基三氟硼酸酯与芳基-和杂芳基三氟甲磺酸酯的I.Suzuki-Miyaura反应。二。含羟基的三氟硼酸盐的氧化。三，三氟硼硼酸同戊烯酸钾的Suzuki-Miyaura反应。 IV。研发有机三氟硼酸盐的HRMS方法
6. Computationally Assisted Mechanistic Investigation and Development of Pd-Catalyzed Asymmetric Suzuki-Miyaura and Negishi Cross-Coupling Reactions for Tetra-ortho-Substituted Biaryl Synthesis [O] . Nitinchandra Dahyabhai Patel, Joshua D. Sieber, Sergei Tcyrulnikov, -1

机译：Pd催化的不对称Suzuki-Miyaura和Neshishi交叉偶联反应的计算辅助机理研究与开发用于四邻位取代联芳基的合成
7. Synthesis of stereodefined 1-aryl(heteroaryl) substituted 1,2-bis(2-bromopyridin-3-yl)ethenes by selective tandem Suzuki-Miyaura\ud Cross-coupling reactions [O] . Baldino, Salvatore, Chelucci, Giorgio Adolfo 2008

机译：选择性串联Suzuki-Miyaura \ ud合成立体定义的1-芳基（杂芳基）取代的1,2-双（2-溴吡啶-3-基）乙烯交叉偶联反应
8. Phase Transfer Pd(O) Catalyzed Polymerization Reactions. 1. Synthesis of 1,2-(4,4'-Dialkoxyaryl)Acetylene Monomers and 1,4-Bis(2-(4',4''-Dialkoxyphenyl)Ethynyl)Benzene Derivatives by Phase Transfer Pd(O)/Cu(I) Catalyzed Coupling Reactions. [R] . Pugh, C., Percec, V. 1990

机译：相转移pd（O）催化的聚合反应。 1.相转移pd（O）/ Cu合成1,2-（4,4'-二烷氧基芳基）乙炔单体和1,4-双（2-（4'，4'-二烷氧基苯基）乙炔基）苯衍生物（I）催化的偶联反应。

Synthesis of stereodefined 1-aryl(heteroaryl) substituted 1,2-bis(2-bromopyridin-3-yl)ethenes by selective tandem Suzuki-Miyaura cross-coupling reactions

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