AIBN-promoted amidation of anilines with 1, 3-diketones via oxidative cleavage of C-C bond under aerobic conditions

Rao Sadu Nageswara; Mohan Darapaneni Chandra; Adimurthy Subbarayappa

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AIBN-promoted amidation of anilines with 1, 3-diketones via oxidative cleavage of C-C bond under aerobic conditions

机译：AIBN通过好氧条件下C-C键的氧化裂解促进苯胺与1，3-二酮的酰胺化

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摘要

N-Acylation of anilines with 1, 3-diketones promoted by AIBN (2-2'-azoisobutyronitrile) under metal free and peroxide-free conditions in the presence of molecular oxygen as oxidant has been described. This protocol proceeds by the oxidative cleavage of C-C bond with simultaneous intermolecular C-N bond formation under mild conditions. (C) 2016 Elsevier Ltd. All rights reserved.

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《Tetrahedron》 |2016年第32期|共6页
作者
Rao Sadu Nageswara; Mohan Darapaneni Chandra; Adimurthy Subbarayappa;
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正文语种 eng
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Acylation; Anilines; 1; 3-Diketones; Amide synthesis; Selective cleavage;

机译：酰化;苯胺;1;3-二酮;酰胺合成;选择性裂解;

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专利

1. AIBN-promoted amidation of anilines with 1, 3-diketones via oxidative cleavage of C-C bond under aerobic conditions [J] . Rao Sadu Nageswara, Mohan Darapaneni Chandra, Adimurthy Subbarayappa Tetrahedron . 2016,第32期

机译：AIBN通过好氧条件下C-C键的氧化裂解促进苯胺与1，3-二酮的酰胺化
2. H2O2-mediated oxidative formation of amides from aromatic amines and 1,3-diketones as acylation agents via C-C bond cleavage at room temperature in water under metal-free conditions [J] . Xi Sun, Min Wang, Pinhua L Green chemistry . 2013,第12期

机译：H2O2介导的芳香族胺和1,3-二酮作为酰化剂在室温下于水中在无金属条件下通过C-C键裂解形成酰胺氧化反应
3. Cu-catalyzed aerobic oxidative amidation of aryl alkyl ketones with azoles to afford tertiary amides via selective C-C bond cleavage [J] . Wen Dinga, Qiuling Song Inorganic Chemistry Frontiers . 2015,第7期

机译：铜催化芳基烷基酮与唑类的好氧氧化酰胺化反应，通过选择性的C-C键断裂提供叔酰胺
4. Indium-Catalyzed Synthesis of Esters from 1,3-Diketones and Alcohols via C-C Bond Cleavage [C] . Atsushi Kawata, Kazumi Takata, Yoichiro Kuninobu Symposium on Organometallic Chemistry . 2007

机译：通过C-C键裂解铟催化1,3-二酮和醇的酯合成酯
5. Making and breaking C-C bonds: Development of enantioselective Diels-Alder and oxidative cleavage reactions. [D] . Payette, Joshua Nathaniel. 2010

机译：建立和打破C-C键：对映选择性Diels-Alder和氧化裂解反应的发展。
6. A Simple Procedure for C-C Bond Cleavage of Aromatic and Aliphatic Epoxides with Aqueous Sodium Periodate Under Ambient Conditions [O] . Caitlin M. Binder, Darryl D. Dixon, Erik Almaraz, -1

机译：在环境条件下用高碘酸钠水溶液进行芳族和脂族环氧的C-C键裂解的简单程序
7. Unexpected C-C Bond Cleavage and C-C Bond Formation Observed in the Reaction of a Cationic Iridium Complex with Heteroatom-Substituted Cyclopropanes [O] . -1

机译：在阳离子铱络合物与杂原子取代的环丙烷的反应中观察到意外的C-C键切割和C-C键形成

AIBN-promoted amidation of anilines with 1, 3-diketones via oxidative cleavage of C-C bond under aerobic conditions

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