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Low temperature synthesis of ZnO nanorods by using PVP and their characterization

机译:PVP低温合成ZnO纳米棒及其表征

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ZnO nanorods are prepared in large quantity at low temperature by using zinc acetate dehydrate and polyvinyl pyrrolidone (PVP) as precursor and capping, respectively. Dependency of morphology and diameter of ZnO nanorods on solvent polarity are investigated. It is observed that diameter of nanorods diminishes with reduction of the solvent polarity. The optical properties of the ZnO nanorods are investigated by UV-Vis spectroscopy. There is a blue-shift in the band-edge with changing of the solvent polarity. The influence of water value on the morphology and diameter of the ZnO nanorods is examined. It is shown that diameter of nanorods decreases by lessening water value; also a blue-shift is observed with decreasing diameter. Effect of Zn/PVP ratio on the ZnO nanorods arrangement is studied.
机译:ZnO纳米棒在低温下分别以醋酸锌脱水和聚乙烯吡咯烷酮(PVP)为前驱体并进行封端制备。研究了ZnO纳米棒的形貌和直径对溶剂极性的依赖性。观察到纳米棒的直径随着溶剂极性的减小而减小。 ZnO纳米棒的光学性质通过紫外-可见光谱研究。随着溶剂极性的改变,带边缘发生蓝移。研究了水分值对ZnO纳米棒的形貌和直径的影响。结果表明,纳米棒的直径随着水值的降低而减小。随着直径的减小,还观察到蓝移。研究了Zn / PVP比对ZnO纳米棒排列的影响。

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