FeCl3/TMSCl: An effective catalytic system for the conjugate addition of sodium p-toluenesulfinate to alpha,beta-enones

Sreedhar B; Reddy MA; Reddy PS

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FeCl3/TMSCl: An effective catalytic system for the conjugate addition of sodium p-toluenesulfinate to alpha,beta-enones

机译：FeCl3 / TMSCl：一种有效的催化体系，用于将对甲苯磺酸钠共轭添加到α，β-烯酮中

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摘要

A new protocol for the beta-sulfination of alpha,beta-unsaturated carbonyl compounds is described. The method employs FeCl3 as catalyst and TMSCl as additive for conjugate addition of sodium p-toluenesulfinate to enones.

机译：描述了一种用于α，β-不饱和羰基化合物的β-硫化的新方案。该方法使用FeCl 3作为催化剂，并使用TMCSI作为添加剂，以将对甲苯磺酸钠共轭加成至烯酮中。

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《Synlett》 |2008年第13期|共4页
作者
Sreedhar B; Reddy MA; Reddy PS;
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正文语种 eng
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beta-sulfonyl ketones; conjugate addition; alpha; beta-unsaturated carbonyl compounds; iron(III) chloride; trimethylsilyl chloride; GRIGNARD REAGENTS; SYNTHETIC APPLICATIONS; SULFONES; EFFICIENT; IRON; HALIDES;

机译：β-磺酰基酮;共轭加成;α;β-不饱和羰基化合物;氯化铁（III）;三甲基甲硅烷基氯;试剂;合成应用;砜;高效;铁;卤化物;

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1. FeCl3/TMSCl: An effective catalytic system for the conjugate addition of sodium p-toluenesulfinate to alpha,beta-enones [J] . Sreedhar B, Reddy MA, Reddy PS Synlett . 2008,第13期

机译：FeCl3 / TMSCl：一种有效的催化体系，用于将对甲苯磺酸钠共轭添加到α，β-烯酮中
2. Asymmetric activation of tropos catalysts in the stereoselective catalytic conjugate additions of R2Zn to alpha,beta-enones: an efficient synthesis of (-)-muscone [J] . Scafato P, Cunsolo G, Labano S, Tetrahedron . 2004,第40期

机译：R2Zn的立体选择性催化共轭加成中的tropos催化剂的不对称活化：α-β-烯酮的有效合成
3. A NEW CATALYTIC ACTIVITY OF ANTIMONY(III) CHLORIDE IN PALLADIUM(0)-CATALYZED CONJUGATE ADDITION OF AROMATICS TO ALPHA,BETA-UNSATURATED KETONES AND ALDEHYDES WITH SODIUM TETRAPHENYLBORATE AND ARYLBORONIC ACIDS [J] . Cho CS., Ohe K., Uemura S., The Journal of Organic Chemistry . 1995,第4期

机译：四溴化硼酸钠和芳烃硼酸在钯（0）催化的芳香族化合物与α-，β-不饱和酮和醛的芳香族共轭加成反应中的氯化锑（III）的新催化活性
4. Catalytic Enantioselective Conjugate Addition of Diethylzinc to A-Alkylidene Esters and Application to Scalable Synthesis of Hiv Protease Inhibitor Tipranavir* [C] . Ma Junan, Wang Lian, Nie Jing Proceedings of international symposium on crystal engineering and drug delivery system 2009 . 2009

机译：二乙基锌在A-亚烷基酯上的催化对映选择性共轭加成反应及其在Hiv蛋白酶抑制剂Tipranavir的可扩展合成中的应用*
5. New methods for catalytic enantioselective conjugate addition of dialkylzinc reagents to alpha,beta-unsaturated carbonyls: Discovery and use of new catalysts. [D] . Hird, Alexander William. 2006

机译：将二烷基锌试剂催化对映选择性共轭加成至α，β-不饱和羰基的新方法：发现和使用新催化剂。
6. Alpha Olefins as Alkenylmetal Equivalents in Catalytic Conjugate Addition Reactions [O] . Dr. Chun-Yu Ho, Dr. Hirohisa Ohmiya, Prof. Dr Timothy F. Jamison -1

机译：Alpha烯烃作为催化共轭加成反应中的烯基金属当量
7. Phosphoramidites: Marvellous ligands in catalytic asymmetric conjugate addition:Marvellous Ligands in Catalytic Asymmetric Conjugate Addition [O] . Feringa B.L. 2000

机译：亚磷酰胺：催化不对称共轭物加成中的奇异配体：催化不对称共轭物加成中的奇异配体

FeCl3/TMSCl: An effective catalytic system for the conjugate addition of sodium p-toluenesulfinate to alpha,beta-enones

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