Unexpected Synthesis of 5,6-Dihydropyridin-2(1H)-ones by a Domino Ugi/Aldol/Hydrolysis Reaction Starting from Baylis-Hillman Phosphonium Saks

Zeng Xiao-Hua; Wang Hong-Mei; Ding Ming-Wu

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Unexpected Synthesis of 5,6-Dihydropyridin-2(1H)-ones by a Domino Ugi/Aldol/Hydrolysis Reaction Starting from Baylis-Hillman Phosphonium Saks

机译：从Baylis-Hillman Sa开始的Domino Ugi / Aldol /水解反应意外合成5,6-Dihydropyridin-2（1H）-ones

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A one-pot synthetic approach to 5,6-dihydropyridin-2(1H)-ones has been developed using a domino process involving Ugi, aldol, and hydrolysis reactions, starting with Baylis-Hillman phosphonium salts, primary amines, isocyanides, and arylglyoxals.

机译：使用涉及Ugi，醛醇缩醛和水解反应的多米诺法，从Baylis-Hillman nium盐，伯胺，异氰化物和芳基乙二醛开始，开发了一种锅法合成5,6-二氢吡啶-2（1H）-酮的方法。。

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《Organic letters》 |2015年第9期|共4页
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Zeng Xiao-Hua; Wang Hong-Mei; Ding Ming-Wu;
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1. Unexpected Synthesis of 5,6-Dihydropyridin-2(1H)-ones by a Domino Ugi/Aldol/Hydrolysis Reaction Starting from Baylis-Hillman Phosphonium Saks [J] . Zeng Xiao-Hua, Wang Hong-Mei, Ding Ming-Wu Organic letters . 2015,第9期

机译：从Baylis-Hillman Sa开始的Domino Ugi / Aldol /水解反应意外合成5,6-Dihydropyridin-2（1H）-ones
2. Reactions of Lithiated Allenes with Isothiocyanates:First Example of Hydrolysis of 2,3-Dihydropyridines as a Novel Synthetic Route to 5,6-Dihydropyridin-2(1H)-ones [J] . N.A.Nedolya, A.I.Albanov, L.V.Klyba, Russian Journal of Organic Chemistry . 2006,第3期

机译：锂化异戊烯与异硫氰酸酯的反应：2,3-二氢吡啶水解为5,6-二氢吡啶-2（1H）-ones的新型合成路线的第一个例子
3. Synthesis of 5,6-Dihydropyridin-2(1H)-ones, 1,5,6,8,8a-Hexa-hydroisoquinolin-3(2H)-ones and 4a,5,6,7,8,8a-Hexahydro-quinolin-2(1H)-ones by Intramolecular Wittig Reaction [J] . Alexander S. Fisyuk Molecules . 2002,第2期

机译：5,6-二氢吡啶-2（1H）-one，1,5,6,8,8a-六氢加氢异喹啉-3（2H）-one和4a，5,6,7,8,8a-六氢-合成分子内维蒂希反应合成喹啉-2（1H）-一
4. An Asymmetric Organocatalytic Domino-Michael-Aldol Reaction [C] . Alexander Kuenkel, Francisco Tato, Magnus Rueping European Symposium on Organic Chemistry . 2009

机译：不对称有机催化多米诺 - Michael-aldol反应
5. Part I. Application of 2-hydroxymethylacrylic acid, a product of Baylis-Hillman reaction, for the synthesis of novel N-backbone-to-side-chain cyclic peptide analogs: Strategies and side reactions. Part II. Synthesis and biological activities of chimeric bioactive peptides featuring amino acids coupled to 4-anilino-n-phenethyl-piperidine. [D] . Petrov, Ravil Rashitovich. 2007

机译：第一部分。Baylis-Hillman反应产物2-羟甲基丙烯酸在合成新型N骨架至侧链环状肽类似物中的应用：策略和副反应。第二部分具有与4-苯胺基-n-苯乙基-哌啶偶联的氨基酸的嵌合生物活性肽的合成和生物活性。
6. One-pot Synthesis of Lactams Using Domino Reactions: Combination of Schmidt Reaction with Sakurai and Aldol Reactions [O] . Chan Woo Huh, Gagandeep K. Somal, Christopher E. Katz, -1

机译：使用多米诺反应的内酰胺的单壶合成：Schmidt与Sakurai和Aldol反应的组合
7. Synthesis of 5,6-Dihydropyridin-2(1H)-ones, 1,5,6,8,8a-Hexahydroisoquinolin-3(2H)-ones and 4a,5,6,7,8,8a-Hexahydroquinolin-2(1H)-ones by Intramolecular Wittig Reaction [O] . Nikolai V. Poendaev, Alexander S. Fisyuk 2002

机译：5,6-二氢吡啶-2（1H）-one，1,5,6,8,8a-六氢异喹啉-3（2H）-one和4a，5,6,7,8,8a-六氢喹啉-2（ 1H）-通过分子内维蒂希反应

Unexpected Synthesis of 5,6-Dihydropyridin-2(1H)-ones by a Domino Ugi/Aldol/Hydrolysis Reaction Starting from Baylis-Hillman Phosphonium Saks

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