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Synthesis of micro/mesoporous silica using poly(ethylene glycol) as a template

机译:以聚乙二醇为模板合成微孔/中孔二氧化硅

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摘要

Analysis of isotherms of low-Temperature nitrogen adsorption-desorption has revealed the for- mation of a micro/mesoporous structure in silica resulting from the sol-gel transition of SiO2 in the presence of poly(ethylene glycol)s with different molecular masses used as templates. The specific surface area of pores has been determined by the BET and Langmuir methods; the volume and surface area of micropores have been estimated by the t-plot method; and the surface area and volume of pores, mesopore size distribution, and average pore diameter have been assessed using the Barrett-Joyner-Halenda method.
机译:对低温氮吸附-解吸等温线的分析表明,在存在不同分子量的聚乙二醇的情况下,SiO 2的溶胶-凝胶转变导致了二氧化硅中微/中微结构的形成。模板。孔的比表面积已通过BET和Langmuir方法确定;微孔的体积和表面积通过t-图法估算;并使用Barrett-Joyner-Halenda方法评估了孔的表面积和体积,中孔尺寸分布以及平均孔径。

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