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Preparation, Microstructure and Photocatalytic Performance of the Anatase Nano-TiO2 Thin Film

机译:锐钛矿型纳米TiO2薄膜的制备,微结构和光催化性能

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摘要

The anatase nano-TiO2 thin films with different layers were prepared on the ordinary glass slides using sol-gel method. The photocatalytic activity of the thin films and the microstructure were investigated. The results showed that the optimum annealing temperature for anatase nano-TiO2was 500 ℃ and TiO2 particles were spherical in shape and dispersed uniformly on the surface of the thin films. The films have good adhesion with the glass substrate. Moreover, the nano-TiO2 particles on the surface have the trend to grow large with the increase of film layers. The prepared thin films have good light transmission rate and the absorption threshold has an obvious red shift with the increase of film layers. Furthermore, the thin films have high photocatalytic activity and the photocatalytic decolourkation rate of acidic black 10B can reach 80 % in 120 min over 6-layer thin film.
机译:采用溶胶-凝胶法在普通载玻片上制备了不同层的锐钛矿型纳米TiO2薄膜。研究了薄膜的光催化活性和微观结构。结果表明,锐钛矿型纳米TiO2的最佳退火温度为500℃,TiO2颗粒呈球形,均匀分散在薄膜表面。所述膜与玻璃基板具有良好的粘附性。而且,随着膜层的增加,表面上的纳米TiO 2颗粒具有增大的趋势。所制备的薄膜具有良好的透光率,并且随着膜层的增加,吸收阈值具有明显的红移。此外,该薄膜具有较高的光催化活性,在六层薄膜上,酸性黑10B在120分钟内的光催化脱色率可达到80%。

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