GREEN PROTOCOL: SOLVENT- AND CATALYST-FREE SYNTHESIS OF BENZIMIDAZOLE DERIVATIVES via MICROWAVE TECHNIQUE

E. Mentese; Ι. S. Dogan; B. Kahveci

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GREEN PROTOCOL: SOLVENT- AND CATALYST-FREE SYNTHESIS OF BENZIMIDAZOLE DERIVATIVES via MICROWAVE TECHNIQUE

机译：绿色协议：通过微波技术合成无溶剂和催化剂的苯并咪唑衍生物

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A simple and green protocol has been developed for the synthesis of benzimidazoles. In this protocol, 2-[(alkyl/aryl)(ethoxy)methylidene]hydrazinecarboxylates with 1,2-phenyle-nediamine derivatives under solvent- and catalyst-free conditions under microwave irradiation lead to the products with good yields in short reaction times.

机译：已经开发了用于合成苯并咪唑的简单且绿色的方案。在该方案中，在无溶剂和催化剂的条件下，微波辐射下2-[（（烷基/芳基）（乙氧基）亚甲基]肼甲酸与1,2-苯基-二胺衍生物与羧酸盐反应，可在较短的反应时间内获得良好的收率。

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《Химия гетероциклических соединений: Всесоюз. науч. теорет. журн.》 |2013年第8期|共5页
作者
E. Mentese; Ι. S. Dogan; B. Kahveci;
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正文语种 eng
中图分类 54.556;
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2-(alkyl/aryl)(ethoxy)methylidenehydrazinecarboxylate; 2-substituted benzimidazole; catalyst-free reaction; microwaves; solvent-free reaction;

机译：2-[（烷基/芳基）（乙氧基）亚甲基]肼甲酸甲酯;2-取代的苯并咪唑;无催化剂反应;微波;无溶剂反应;

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专利

1. Green protocol: Solvent- and catalyst-free synthesis of benzimidazole derivatives via microwave technique [J] . Mente?e E., Do?an I.S., Kahveci B. Chemistry of heterocyclic compounds . 2013,第8期

机译：绿色方案：通过微波技术无溶剂和无催化剂地合成苯并咪唑衍生物
2. Green methodologies in organic synthesis: Microwave assisted solvent- and catalyst-free synthesis of enaminones and their conversion into 1,3,5-trisubstituted benzenes as well as 3-aroyl-6-substituted pyridines [J] . Morsy Ahmed El-Apasery, Saleh Mohamed Al-Mousawi, Mohamed Helmy Elnagdi European Journal of Chemistry . 2011,第2期

机译：有机合成中的绿色方法：微波辅助的无溶剂和无催化剂的烯胺酮合成及其转化为1,3,5-三取代的苯以及3-芳基-6取代的吡啶
3. A General Protocol for the Solvent- and Catalyst-Free Synthesis of 2-Styrylquinolines under Focused Microwave Irradiation [J] . Matteo Staderini, Nieves Cabezas, Maria Laura Bolognesi, Synlett . 2011,第17期

机译：聚焦微波辐射下无溶剂和无催化剂合成2-苯乙烯基喹啉的通用方案
4. Comparison of Conventional and Microwave-assisted Synthesis of Benzimidazole Derivative from CitronellaI in Kaffir lime oil (Citrus hystrix DC.) [C] . W Warsito, Noorhamdani A.S, Suratmo Joint Conference on Chemistry . 2018

机译：康西尔石灰油中康西唑达苯并咪唑衍生物的常规和微波辅助合成的比较（柑橘Hystrix DC。）
5. New developments toward the synthesis of heterocycles and applications in green chemistry. I. A simple and essentially one-pot synthesis of N-aminated heterocycles using phase transfer catalyst (Aliquat-336). II. Synthesis of pharmaceutically important pyrrole derivatives. III. Applications in green chemistry: Surfactant-mediated environmentally friendly cleavage of aromatic esters and trans-esterification under solvent-free neutral conditions . [D] . Patel, Nitinchandra. 2005

机译：杂环合成的新进展及其在绿色化学中的应用。 I.使用相转移催化剂（Aliquat-336）简单且基本上一锅合成N-胺化的杂环。二。药学上重要的吡咯衍生物的合成。三，在绿色化学中的应用：在无溶剂的中性条件下，表面活性剂介导的环境友好的芳族酯裂解和酯交换反应。
6. Solvent- and Catalyst-Free One-Pot Green Bound-TypeFused Bis-Heterocycles Synthesis via Groebke–Blackburn–BienayméReaction/SNAr/Ring-Chain Azido-Tautomerization Strategy [O] . MiguelÁngel Claudio-Catalán, Shrikant G. Pharande, Andrea Quezada-Soto, 2018

机译：不含溶剂和催化剂的一罐绿色粘合剂Groebke–Blackburn–Bienaymé的熔融双杂环合成反应/ SNAr /环链叠氮基互变异构策略
7. Microwave assisted solvent-, support- and catalyst-free synthesis of enaminones [O] . Carlos Kleber Z. Andrade, Angélica de Fátima S. Barreto, Wender A. Silva 2008

机译：微波辅助溶剂，无载体和催化剂的烯胺酮合成

GREEN PROTOCOL: SOLVENT- AND CATALYST-FREE SYNTHESIS OF BENZIMIDAZOLE DERIVATIVES via MICROWAVE TECHNIQUE

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