Microwave assisted synthesis of hydroxychromenes using imidazole-functionalized silica nanoparticles as a catalyst under solvent-free conditions

摘要

A microwave-assisted reaction of various salicylaldehydes with dialkyl acetylenedicarboxylates mediated by imidazole-functionalized silica nanoparticles is successfully and rapidly achieved to afford the corresponding hydroxychromenes in high to excellent yields under solvent-free conditions. (C) 2015 Academie des sciences. Published by Elsevier Masson SAS. All rights reserved.