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Microstructures and Mechanical Properties of (NiAl+Ni_3Al) Two-Phase Intermetallic Compounds Produced by MA-HIP Process

机译:MA-HIP法制备(NiAl + Ni_3Al)两相金属间化合物的组织和力学性能

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摘要

The (Ni_3Al+NiAl) intermetallic compounds were produced by MA-HIP method. There are two cases for the sintered specimens; the one was produced using only elemental powders (EP specimen) and the other was produced using both NiAl prealloyed and nickel powders (PP specimen). Those alloys were subjected to the heat refining process. The microstructural change and mechanical properties were investigated. It was found that the fine particles with the size of less than 3#mu#m were obtained by MA process. EP specimen showed very fine microstructures with almost full density. On the other hand, PP specimens showed higher relative density with increasing HIP temperature. After heat-refining treatment, EP specimen had fine structure, since the size of the prior #beta# grains and the width of lamella decreased comparing with PP specimens. There was the tendency for the mechanical properties of PP specimens to approach those of EP specimen with increasing HIP temperature. The strain rate sensitivity exponent, m value, was found to be about 0.52 for EP specimen and 0.34 for PP specimen at 1073K. This high m value suggests the occurrence of superplastic deformation especially in EP specimen.
机译:通过MA-HIP法制备了(Ni_3Al + NiAl)金属间化合物。烧结样品有两种情况。一种仅使用元素粉末(EP试样)生产,另一种同时使用NiAl预合金和镍粉(PP试样)生产。那些合金经过了热精炼工艺。研究了组织变化和力学性能。发现通过MA工艺获得了尺寸小于3#μm的细颗粒。 EP样品显示出非常精细的微结构,几乎充满了密度。另一方面,随着HIP温度的升高,PP样品显示出较高的相对密度。经过热处理后,EP试样具有良好的结构,因为与PP试样相比,先前的#beta#晶粒的尺寸和薄片的宽度减小了。随着HIP温度的升高,PP试样的机械性能趋向于接近EP试样。发现在1073K时,EP样品的应变速率灵敏度指数m值约为0.52,PP样品的应变速率灵敏度指数m值为0.34。这个高的m值表明发生了超塑性变形,特别是在EP试样中。

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