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Simultaneous Measuring Method of Thermal Properties for Thermoelectric Materials

机译:热电材料热性能的同时测量方法

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In order to grasp the various thermal properties for the thermoelectric materials such as Bi_2 Te_3 and PbTe, the novel technique has been developed using an identical specimen with the unchanged experimental set-up. The new design principle based on Angstrom's method employs the as heat source to give a specimen the periodical temperature oscillation and its phase shift. Since the dc one is also still available, it is feasible to perform the combination and simultaneous measurement of thermals diffusivity a and heat capacity c_p as well as thermal conductivity k. Actually, the measurements were carried out sing a transparent quartz glass, which is commonly used as reference material in measuring k for thermoelectric materials especially for Bi_2Te_3 materials. a obtained is in quite good agreement with the literature value at room temperature. Also by the aid of c_p-values obtained through ac calorimetric method the validity and reliability of temperature dependence of a was verified.
机译:为了掌握诸如Bi_2 Te_3和PbTe之类的热电材料的各种热性能,已使用相同的试样开发了一种新颖的技术,其实验设置没有改变。基于Angstrom方法的新设计原理采用热源为样本提供周期性的温度振荡及其相移。由于dc仍然可用,因此可以同时进行热扩散系数a和热容c_p以及热导率k的组合测量。实际上,使用透明石英玻璃进行测量,该透明石英玻璃通常用作热电材料特别是Bi_2Te_3材料的k测量中的参考材料。所获得的值与室温下的文献值非常吻合。同样借助于借助于量热法获得的c_p值,证实了α的温度依赖性的有效性和可靠性。

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