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Preparation and antibacterial activity of silver-doped organic-inorganic hybrid coatings on glass substrates

机译:玻璃基底上掺银有机-无机杂化涂层的制备及抑菌活性

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摘要

Silver-doped organic-inorganic hybrid coating solutions were prepared by incorporating AgNO3 into organic-inorganic hybrid sols derived from methacryloxypropyl trimethoxysilane (MEMO) and vinyltriethoxysilane (VTES) using the sol-gel method. They were applied on the soda-lime slide glass, and crack-free and transparent coatings were obtained by a low temperature heat treatment at 150 degrees C for 3 h. The formation of Ag colloids in the coating films was confirmed by UV-vis spectroscopy and scanning electron microscopy. The size control of Ag colloids in the coating films was possible by adjusting initial AgNO3 concentrations in the coating solutions. The antibacterial activity of the coating films was tested against Gram-positive Staphylococcus aureus and Gram-negative Escherichia coli bacteria by film contact method. The coating films exhibited an excellent antibacterial activity against both S. aureus and E. coli.
机译:通过使用溶胶-凝胶法将AgNO3掺入衍生自甲基丙烯酰氧基丙基三甲氧基硅烷(MEMO)和乙烯基三乙氧基硅烷(VTES)的有机-无机杂化溶胶中,制备了掺银的有机-无机杂化涂料溶液。将它们涂覆在钠钙载玻片上,并通过在150摄氏度下进行3小时的低温热处理获得了无裂纹和透明的涂层。通过UV-可见光谱和扫描电子显微镜确认涂膜中Ag胶体的形成。通过调节涂料溶液中的初始AgNO3浓度,可以控制涂膜中Ag胶体的尺寸。通过膜接触法测试了涂膜对革兰氏阳性金黄色葡萄球菌和革兰氏阴性大肠杆菌的抗菌活性。涂膜对金黄色葡萄球菌和大肠杆菌均表现出优异的抗菌活性。

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