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Effects of electrophoretic deposition parameters on the photocatalytic activity of TiO_2 films: Optimization by response surface methodology

机译:电泳沉积参数对TiO_2薄膜光催化活性的影响:响应面法优化

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摘要

In this work, the electrophoretic deposition method was utilized to immobilize TiO2 particles on stainless steel substrates. In addition, for the first time, statistics-based experimental design using response surface methodology was employed to investigate the effect of four key coating parameters (i.e. applied voltage, calcination temperature, photocatalyst weight percentage, and deposition time) on the photocatalytic degradation. Analysis of variance revealed that the proposed model was adequate. X-ray diffraction and scanning electron microscope were used to evaluate the effects of the parameters on degradation efficiency. The optimum applied voltage, calcination temperature, catalyst concentration and deposition time were found to be 25 V, 300°C, 1.0 wt%, and 300 s, respectively. Under these conditions, the degradation efficiency reached 85.88%.
机译:在这项工作中,利用电泳沉积方法将TiO2颗粒固定在不锈钢基板上。此外,首次采用基于响应表面方法的基于统计的实验设计来研究四个关键涂层参数(即施加电压,煅烧温度,光催化剂重量百分比和沉积时间)对光催化降解的影响。方差分析表明,提出的模型是足够的。 X射线衍射和扫描电子显微镜被用来评估参数对降解效率的影响。最佳施加电压,煅烧温度,催化剂浓度和沉积时间分别为25 V,300°C,1.0 wt%和300 s。在这些条件下,降解效率达到了85.88%。

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