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首页> 外文期刊>Journal of the European Ceramic Society >In situ hot pressing/reaction synthesis, mechanical and thermal properties of Lu_2SiO_5
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In situ hot pressing/reaction synthesis, mechanical and thermal properties of Lu_2SiO_5

机译:原位热压/反应合成Lu_2SiO_5的力学和热学性能

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摘要

Lu_2SiO_5 is a promising candidate of environmental barrier coatings (EBC) for silicon based ceramics due to its excellent high temperature stability. However, little information is available for the mechanical and thermal properties of Lu_2SiO_5, which frustrated evaluation of its performances for EBC applications. In this paper, dense Lu2SiC>5 ceramic is successfully fabricated from Lu_2O_3 and SiO_2 powders by in situ hot pressing/reaction sintering at 1500 °C. Mechanical properties, including Young's modulus, bulk modulus, shear modulus, Poisson's ratio, fracture toughness, Vickers hardness, and bending strength are reported for the first time. Lu_2SiO_5 possesses excellent high temperature mechanical properties up to at least 1300 °C. Thermal stress for the case of Lu_2SiO_5 or Y_2SiO_5 coating on silicon bond coat and thermal stress resistance parameter are also estimated based on the experimental mechanical and thermal properties. The present results suggest that Lu_2SiO_5 has better reliability than Y_2SiO_5 in harsh thermal environment.
机译:Lu_2SiO_5由于其出色的高温稳定性,因此是用于硅基陶瓷的环境屏障涂层(EBC)的有希望的候选者。然而,关于Lu_2SiO_5的机械和热学性质的信息很少,这挫伤了其在EBC应用中的性能评估。本文通过在1500°C下进行原位热压/反应烧结,成功地由Lu_2O_3和SiO_2粉末制备了致密的Lu2SiC> 5陶瓷。首次报告了机械性能,包括杨氏模量,体积模量,剪切模量,泊松比,断裂韧性,维氏硬度和抗弯强度。 Lu_2SiO_5在至少1300°C的温度下具有出色的高温机械性能。还基于实验的机械和热性能,估算了在硅粘结涂层上涂Lu_2SiO_5或Y_2SiO_5时的热应力和抗热应力参数。目前的结果表明,在恶劣的热环境下,Lu_2SiO_5具有比Y_2SiO_5更好的可靠性。

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