首页> 外文期刊>Journal of Sol-Gel Science and Technology >Preparation and characterization of In2O3/ZnO heterostructured microbelts by sol-gel combined with electrospinning method
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Preparation and characterization of In2O3/ZnO heterostructured microbelts by sol-gel combined with electrospinning method

机译:溶胶-凝胶结合电纺丝法制备In2O3 / ZnO异质微带及其表征

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摘要

Long and thin In2O3/ZnO heterostructured microbelts were synthesized by sol-gel combined with electrospinning process. The as-prepared microbelts show the weir defined one-dimensional belt structures with 1-5-urn in width and tens of millimeters in length. The polycrys-talline microbelts calcined at 973 K for 1 h are still continuous and have the uniform rectangular cross sections and the thickness to width ratio is around 1:10. The crystalline phases of samples are investigated by X-ray diffraction and the morphology is examined using transmission electron microscope and scanning electron microscope. In2O3/ZnO heterostructured microbelts exhibit the excellent visible photocatalytic property in the photo-degradation of methyl orange (MO), and over 94 % of MO was degraded within 3 h.
机译:溶胶-凝胶结合静电纺丝法制备了长而细的In2O3 / ZnO异质结构微带。所制备的微带显示出堰限定的一维带状结构,其宽度为1至5 ur,长度为数十毫米。在973 K下煅烧1 h的多结晶滑石微带仍然是连续的,并且具有均匀的矩形横截面,并且厚度与宽度之比约为1:10。通过X射线衍射研究样品的结晶相,并使用透射电子显微镜和扫描电子显微镜检查形态。 In2O3 / ZnO异质结构微带在甲基橙(MO)的光降解中表现出优异的可见光催化性能,超过94%的MO在3小时内降解。

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