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首页> 外文期刊>Journal of optoelectronics and advanced materials >The characterization of surfaces of electro polished 316L stainless steel for orthopedic implant applications
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The characterization of surfaces of electro polished 316L stainless steel for orthopedic implant applications

机译:用于整形外科植入物的电抛光316L不锈钢的表面特性

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摘要

The characterization of the surface of electro polished 316L stainless steel by using poly(O-2-hydroxyethyl) starch (PETA) in physiological serum (PS) is discussed according to electrochemical measurements, scanning electron microscopy and Mossbauer Spectroscopy. The results obtained through polarization curves indicate that critical potential in pitting (E-cp) are shifted to a higher values with the increase in PETA concentration; PETA reduces anodic dissolution and also decrease of the corrosion current (i(corr)). Decrease of the corrosion current (i(corr)) was associated with a shift of corrosion potential (E-corr) to a less negative values. The polarization resistance(R-p) increases for the surfaces which were electro polished in physiological serum in the presence of PETA. Scanning electron microscopy(SEM) shown no evidence of corrosion pits on Surfaces of Electro polished 316L Stainless Steel, but the formation of a thick film on the steel surface was observed. The surface Mossbauer spectrometry proves the uniformity, compactness and stability of the passive films.
机译:根据电化学测量,扫描电子显微镜和莫斯鲍尔光谱技术,讨论了在生理血清(PS)中使用聚(O-2-羟乙基)淀粉(PETA)对电抛光316L不锈钢表面的表征。通过极化曲线获得的结果表明,随着PETA浓度的增加,点蚀的临界电势(E-cp)移至更高的值。 PETA可以减少阳极溶解,还可以降低腐蚀电流(i(corr))。腐蚀电流(i(corr))的减少与腐蚀电位(E-corr)向较小负值的偏移相关。在PETA存在下,在生理血清中进行电抛光的表面的极化电阻(R-p)增加。扫描电子显微镜(SEM)没有发现在电抛光的316L不锈钢表面上有腐蚀坑的迹象,但是观察到在钢表面上形成了厚膜。表面莫斯鲍尔光谱法证明了钝化膜的均匀性,致密性和稳定性。

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