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Simulation of pilot-plant extraction experiments to reduce the aromatic content from lubricating oils

机译:模拟中试工厂提取实验以减少润滑油中的芳烃含量

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摘要

In the lubricating oil manufacturing process, the aromatic content from vacuum distillates is reduced by solvent extraction, frequently with furfural. These mixtures present very complex composition which makes difficult the description of the liquid-liquid equilibrium involved. In previous studies the possibility to describe such equilibrium by using a reduced number of pseudo-components and the NRTL model has been shown. In this generalized model few physical properties of the lubricating oil used as feed are needed as experimental information. In this work, such model was applied to pilot-plant experiments carried out with different lube oils within the range (SPD-HND). The accuracy of the model was checked by simulating multi-stage extractions using AspenPlus. Calculated and experimental yields, and refractive index of the involved mixtures were compared and a good agreement was obtained for the experiments carried out with the heavier lubricating oil cuts.
机译:在润滑油的生产过程中,经常通过糠醛的溶剂萃取减少真空馏出物中的芳烃含量。这些混合物具有非常复杂的组成,这使得难以描述所涉及的液-液平衡。在以前的研究中,已经显示出通过使用减少数量的伪成分和NRTL模型来描述这种平衡的可能性。在此通用模型中,几乎不需要用作进料的润滑油的物理性质作为实验信息。在这项工作中,将这种模型应用于在该范围内使用不同润滑油(SPD-HND)进行的中试实验。通过使用AspenPlus模拟多阶段提取来检查模型的准确性。比较了所计算的和实验的产率以及所涉及混合物的折射率,并且对于使用较重的润滑油馏分进行的实验获得了良好的一致性。

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