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Yield stress measurement of gelled waxy crude oil: Gap size requirement

机译:胶凝蜡状原油的屈服应力测量:间隙尺寸要求

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The strength of gelled waxy crude oil is an important parameter required to determine the restart pressure of pipelines filled with the gelled waxy crude oil. Several measurement methods have been proposed in the literature to quantify the yield strength utilizing a rheometer. Minimal discussions, are however, provided on the effects of rheometer geometry gap on the yield stress measurements. This study is intended to propose a systematic protocol to determine the geometry gap settings for better repeatability of the yield stress measurements of gelled waxy crude oils. The reliability of the yield stress data measured has been shown to be highly dependent on the gap selection in the rheometer. The ten-to-one gap ratio has been proven to be inapplicable for the case of gelled waxy crude oils which consists of wax crystal networks entrapping the oil phase. Presence and strong interactions of large wax crystals presents wall effects and subsequently reduces the repeatability of the measurements. The method proposed in this study has been proven to work on a mild waxy crude oil as well as on a more "severe" waxy crude oil. It can be utilized prior to any transient theological measurements as gap setting is crucial to ensure accurate and reliable measurements. (C) 2015 Elsevier B.V. All rights reserved.
机译:凝胶状蜡质原油的强度是确定填充凝胶状蜡质原油的管道的重启压力所需的重要参数。在文献中已经提出了几种测量方法,以利用流变仪来量化屈服强度。但是,关于流变仪几何间隙对屈服应力测量的影响的讨论最少。这项研究旨在提出一种系统协议,以确定几何间隙设置,以便更好地重复测量胶凝蜡质原油的屈服应力。已经显示,所测量的屈服应力数据的可靠性高度依赖于流变仪中的间隙选择。已经证明十比一的空隙比不适用于凝胶状蜡质原油,该胶状蜡质原油由包裹油相的蜡晶网络组成。大蜡晶体的存在和强烈的相互作用会产生壁效应,从而降低测量的可重复性。这项研究中提出的方法已被证明适用于温和的蜡质原油以及更“严重”的蜡质原油。它可以在任何瞬态神学测量之前使用,因为间隙设置对于确保精确和可靠的测量至关重要。 (C)2015 Elsevier B.V.保留所有权利。

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