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首页> 外文期刊>Journal of Materials Engineering and Performance >Effects of HA-Coating on the Surface Morphology and Corrosion Behavior of a Co-Cr-Based Implant in Different Conditions
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Effects of HA-Coating on the Surface Morphology and Corrosion Behavior of a Co-Cr-Based Implant in Different Conditions

机译:HA涂层对不同条件下Co-Cr基植入物表面形态和腐蚀行为的影响

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摘要

The corrosion behavior and surface morphology of a Co-Cr-based implant after HA-coating using the sol-gel method were investigated. Sintering was performed at four different conditions. Surfaces of the samples were characterized and evaluated using field emission scanning electron microscopy. Atomic force microscope was used to measure the surface roughness and to collect the micrographs of the HA-coating layer. The x-ray diffraction results confirmed the formation of a crystalline phase of HA on the surface of the substrates. To measure the corrosion resistance, the samples were dip-coated with two different thicknesses (78 and 142 mu m), and then tested by potentiodynamic polarization and spectroscopy (EIS) in SBF at 37 degrees C after sintering process. This study revealed that the thickness of the HA-coating layer affects the corrosion rate of the substrate, but the sintering condition of the HA-coating layer plays a remarkably more significant role in improving the corrosion resistance of Co-Cr-based implants. Moreover, the sample sintered at 600 degrees C for 20 min with thickness of 142 mu m showed considerably enhanced surface morphology and superior corrosion resistance compared with the bare material and other treated samples.
机译:研究了使用溶胶-凝胶法进行HA涂层后Co-Cr基植入物的腐蚀行为和表面形态。在四个不同条件下进行烧结。使用场发射扫描电子显微镜对样品的表面进行表征和评估。使用原子力显微镜测量表面粗糙度并收集HA涂层的显微照片。 X射线衍射结果证实了在基材表面上HA的结晶相的形成。为了测量耐腐蚀性,将样品浸涂有两种不同的厚度(78和142μm),然后在烧结后于37摄氏度下在SBF中通过电动力极化和光谱(EIS)测试。这项研究表明,HA涂层的厚度会影响基材的腐蚀速率,但是HA涂层的烧结条件在改善Co-Cr基植入物的耐腐蚀性方面起着更为重要的作用。此外,与裸露的材料和其他处理过的样品相比,在600℃烧结20分钟,厚度为142μm的样品显示出明显增强的表面形态和优异的耐腐蚀性。

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