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Pulse Electrochemical Meso/Micro/Nano Ultraprecision Machining Technology

机译:脉冲电化学中/微/纳米超精密加工技术

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This study demonstrated meso/microano-ultraprecision machining through electrochemical reactions using intermittent DC pulses. The experiment focused on two machining methods: (1) pulse electrochemical polishing (PECP) of stainless steel, and (2) pulse electrochemical nano-patterning (PECNP) on a silicon (Si) surface, using atomic force microscopy (AFM) for fabrication. The dissolution reaction at the stainless steel surface following PECP produced a very clean, smooth workpiece. The advantages of the PECP process included improvements in corrosion resistance, deburring of the sample surface, and removal of hydrogen from the stainless steel surface as verified by time-of-flight secondary-ion mass spectrometry (TOF-SIMS). In PECNP, the electrochemical reaction generated within water molecules produced nanoscale oxide textures on a Si surface. Scanning probe microscopy (SPM) was used to evaluate nanoscale-pattern processing on a Si wafer surface produced by AFM-PECNP. For both processes using pulse electrochemical reactions, three-dimensional (3-D) measurements and AFM were used to investigate the changes on the machined surfaces. Preliminary results indicated the potential for advancing surface polishing techniques and localized microano-texturing technology using PECP and PECNP processes.
机译:这项研究证明了使用间歇性DC脉冲通过电化学反应进行中观/微观/纳米超精密加工。实验着重于两种加工方法:(1)不锈钢的脉冲电化学抛光(PECP),以及(2)使用原子力显微镜(AFM)进行制造的在硅(Si)表面上的脉冲电化学纳米图案(PECNP)。 。 PECP之后,不锈钢表面的溶解反应产生了非常干净,光滑的工件。 PECP工艺的优点包括改进的耐腐蚀性,样品表面的去毛刺以及从不锈钢表面去除氢,这已经通过飞行时间二次离子质谱(TOF-SIMS)进行了验证。在PECNP中,水分子内产生的电化学反应在Si表面产生纳米级氧化物织构。扫描探针显微镜(SPM)用于评估由AFM-PECNP生产的Si晶片表面的纳米级图案加工。对于使用脉冲电化学反应的两个过程,都使用了三维(3-D)测量和AFM来研究机加工表面的变化。初步结果表明,使用PECP和PECNP工艺的表面抛光技术和局部微/纳米纹理技术的发展潜力很大。

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