Study of ancient lead materials: A gallo-roman sarcophagus - contribution of the electrolytic treatment to its restoration

Rocca E.; Mirambet F.; Steinmetz J.

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Study of ancient lead materials: A gallo-roman sarcophagus - contribution of the electrolytic treatment to its restoration

机译：古代铅材料的研究：高卢石棺-电解对其修复的贡献

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The restoration of metallic archaeological artefacts needs the knowledge of ancient materials - their composition, their state of conservation and their manufacturing process - to avoid any inappropriate action in the restoration process. This paper is devoted to the study of a lead gallo-roman sarcophagus, found in a much corroded state after a long burial in a calcareous soil in the banks of the Rhone River at Lyon ( France). From the metallographic observations, it was found that the lead sheets constituting the sarcophagus have been directly cast on a table covered with a bed of sand. In addition, the presence of a thick corrosion layer consisting of lead oxide, lead carbonates and some important penetrations of PbO in the metal explain the loss of lead ductility and the important brittleness of this ancient material. The mechanism of formation and growth of this PbO layer in a carbonated medium was studied using electrochemical experiments and metallographic observations. Finally, the comprehensive study of this complex material consisting of lead metals, a PbO/lead carbonate layer and some compounds of the soil allowed the setting up of a restoration process based on an electrochemical reduction method. (C) 2004 Kluwer Academic Publishers. [References: 21]

机译：金属考古文物的修复需要古代材料的知识-它们的组成，保存状态和制造过程-避免在修复过程中采取任何不适当的行动。本文致力于研究铅制的古罗马石棺，在法国里昂罗纳河两岸的石灰岩土壤中长期埋葬后，处于腐蚀严重的状态。从金相观察中发现，构成石棺的铅片直接浇铸在铺有沙床的桌子上。另外，由氧化铅，碳酸铅和金属中一些重要的PbO渗透组成的厚腐蚀层的存在解释了铅延展性的丧失和这种古老材料的重要脆性。使用电化学实验和金相观察研究了在碳酸介质中该PbO层的形成和生长机理。最后，对这种由铅金属，PbO /碳酸铅层和土壤中某些化合物组成的复杂材料的综合研究，使得可以建立基于电化学还原法的修复过程。（C）2004 Kluwer学术出版社。 [参考：21]

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《Journal of Materials Science》 |2004年第8期|共8页
作者
Rocca E.; Mirambet F.; Steinmetz J.;
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正文语种 eng
中图分类工程材料学;
关键词
Sulfuric-acid; Corrosion; Alloys; Films;

机译：硫酸;腐蚀;合金;薄膜;

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1. Study of ancient lead materials: A gallo-roman sarcophagus - contribution of the electrolytic treatment to its restoration [J] . Rocca E., Mirambet F., Steinmetz J. Journal of Materials Science . 2004,第8期

机译：古代铅材料的研究：高卢石棺-电解对其修复的贡献
2. Unilateral NMR, 13C CPMAS NMR spectroscopy and micro-analytical techniques for studying the materials and state of conservation of an ancient Egyptian wooden sarcophagus [J] . Proietti N., Presciutti F., Di Tullio V., Analytical and bioanalytical chemistry . 2011,第9期

机译：单边NMR，13C CPMAS NMR光谱学和显微分析技术，用于研究古埃及木棺木的材料和保存状态
3. Unilateral NMR, 13C CPMAS NMR spectroscopy and micro-analytical techniques for studying the materials and state of conservation of an ancient Egyptian wooden sarcophagus [J] . Noemi Proietti, Federica Presciutti, Valeria Di Tullio, Analytical and Bioanalytical Chemistry . 2011,第9期

机译：单边NMR， 13 C CPMAS NMR光谱学和显微分析技术，用于研究古埃及木制石棺的材料和保存状态
4. Close relations between metallic materials, heat treatment and thermochemical treatment on the microstructure: contribution of metallographic examinations performed on industrial parts through several case studies [C] . Patrick Jacquot, Bruno Stauder, Nicole Jacquot, International Federation for Heat Treatment and Surface Engineering Congress . 2016

机译：金属材料，热处理与热化学处理与微观结构的密切关系：几种案例研究对工业部位进行的金相检查的贡献
5. Examination of microstructural liquid phase behavior during heat treatment of doped -- lead telluride thermoelectric materials. [D] . Langan, Sean McCoy. 2014

机译：检查掺杂碲化铅热电材料热处理过程中的微观结构液相行为。
6. Bracket bonding to polymethylmethacrylate-based materials for computer-aided design/manufacture of temporary restorations: Influence of mechanical treatment and chemical treatment with universal adhesives [O] . Cecilia Goracci, Mutlu Özcan, Lorenzo Franchi, 2019

机译：支架粘结到基于聚甲基丙烯酸甲酯的材料上用于计算机辅助设计/制造临时修复体：机械处理和化学处理以及通用粘合剂的影响
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Gustav and KnightS. (eds), British Industrial Fictions , University of Wales Press, 2000, pp. viii + 212, £14.99 pb.; BalchJack S., Lamps at High Noon , University of Illinois Press, 2000, pp. xl + 404, $19.45 pb.; ConroyJack, A World to Win , University of Illinois Press, 2000, pp. xxxv + 348, $17.95 pb.GagnierRegenia, The Insatiability of Human Wants: Economics and Aesthetics in Market Society , University of Chicago Press, 2000, pp. 352, £10.50 pb. [O] . Paul Hyland, R. C. Richardson, Ivan Roots, 2001

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Study of ancient lead materials: A gallo-roman sarcophagus - contribution of the electrolytic treatment to its restoration

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