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Experimental studies on comparison of microwave curing and thermal curing of epoxy resins used for alternative mould materials

机译:替代模具材料用环氧树脂的微波固化和热固化比较实验研究

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摘要

In this present work attempts have been made to study the glass transition temperature of alternative mould materials by using both microwave heating and conventional oven heating. In this present work three epoxy resins, namely R2512, R2515 and R2516, which are commonly used for making injection moulds have been used in combination with two hardeners H2403 and H2409. The magnetron microwave generator used in this research is operating at a frequency of 2.45 GHz with a hollow rectangular waveguide. In order to distinguish the effects between the microwave and conventional heating, a number of experiments were performed to test their mechanical properties such as tensile and flexural strengths. Additionally, differential scanning calorimeter technique was implemented to measure the glass transition temperature on both microwave and conventional heating. This study provided necessary evidences to establish that microwave heated mould materials resulted with higher glass transition temperature than the conventional heating. Finally, attempts were also made to study the microstructure of microwave-cured materials by using a scanning electron microscope in order to analyze the morphology of cured specimens.
机译:在本工作中,已经尝试通过使用微波加热和常规烤箱加热来研究替代模具材料的玻璃化转变温度。在本工作中,已将三种常用于制作注塑模具的环氧树脂R2512,R2515和R2516与两种固化剂H2403和H2409结合使用。本研究中使用的磁控管微波发生器使用空心矩形波导以2.45 GHz的频率运行。为了区分微波和常规加热之间的影响,进行了许多实验以测试其机械性能,例如拉伸强度和弯曲强度。另外,采用差示扫描量热仪技术来测量微波和常规加热下的玻璃化转变温度。这项研究提供了必要的证据,证明微波加热的模具材料比常规加热具有更高的玻璃化转变温度。最后,还尝试通过扫描电子显微镜研究微波固化材料的微观结构,以分析固化样品的形态。

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