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Multiple Abnormal Grain Growth Phenomena in Nanocrystalline Pure Nickel Produced by Electrodeposition

机译:电沉积法制备纳米晶纯镍中的多个异常晶粒生长现象

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摘要

Here we show multiple abnormal grain growth phenomena in nanocrystalline pure Ni with temperature change, based on the microstructural analysis. Abnormally large grains are observed in the nanocrystalline Ni thermally exposed in air for 1 hr at 200 deg C, 500 deg C, and 800 deg C, respectively. Such large grains formed at 500 deg C for 1 hr having facet grain boundary structure, show kinetically fast growth rate rather than others exposed to 200 deg C and 800 deg C for the same time period. The facet grain boundary appears to be related to the abnormal grain growth rate, suppressing the fine matrix grain growth. The mechanism underlying abnormal grain growth is examined for each temperature range.
机译:在此,基于微观结构分析,我们显示出随着温度变化纳米纯镍中出现多种异常晶粒生长现象。在分别于200℃,500℃和800℃热暴露于空气中1小时的纳米晶Ni中观察到异常大的晶粒。这种具有小晶界结构的,在500摄氏度下持续1个小时形成的大晶粒,显示出动力学上的快速生长速率,而不是其他晶粒同时暴露于200摄氏度和800摄氏度。小面晶界似乎与异常晶粒生长速率有关,从而抑制了基体细晶粒的生长。对于每个温度范围,都检查了异常晶粒长大的潜在机理。

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