Synthesis of boron macrocycles from 1,2-aminoalcohols and 2-formylphenylboronic acid

Appoh FA; Barnes SS; Manning MJ; Turner CS; Vogels CM; Decken A; Westcott SA

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Synthesis of boron macrocycles from 1,2-aminoalcohols and 2-formylphenylboronic acid

机译：由1,2-氨基醇和2-甲酰基苯基硼酸合成硼大环

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Condensation of aminoalcohols with 2-HC(O)C6H4B(OH)(2) afforded the macrocyclic compounds 1 - 7 with an OBOBO structural unit. Crystals of 1 were triclinic, space group P-1, a = 9.9818(12) angstrom, b = 12.8302(15) angstrom, c = 13.1663(15) angstrom, alpha = 105.503(2)degrees, beta = 94.860(2)degrees, gamma = 92.585(2)degrees, Z = 2.

机译：氨基醇与2-HC（O）C6H4B（OH）（2）的缩合得到具有OBOBO结构单元的大环化合物1-7。 1的晶体为三斜晶系，空间群为P-1，a = 9.9818（12）埃，b = 12.8302（15）埃，c = 13.1663（15）埃，alpha = 105.503（2）度，beta = 94.860（2）度，gamma = 92.585（2）度，Z = 2。

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《Journal of Heterocyclic Chemistry: The International Journal of Heterocyclic Chemistry》 |2008年第5期|共4页
作者
Appoh FA; Barnes SS; Manning MJ; Turner CS; Vogels CM; Decken A; Westcott SA;
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正文语种 eng
中图分类有机化学;
关键词
STEREOSELECTIVE ADDITION; ANTIFUNGAL AGENT; C=N BOND; DERIVATIVES; REACTIVITY; COMPLEXES;

机译：立体选择性添加;抗真菌剂;C = N键;衍生物;反应性;络合物;

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1. Synthesis of boron macrocycles from 1,2-aminoalcohols and 2-formylphenylboronic acid [J] . Appoh FA, Barnes SS, Manning MJ, Journal of Heterocyclic Chemistry: The International Journal of Heterocyclic Chemistry . 2008,第5期

机译：由1,2-氨基醇和2-甲酰基苯基硼酸合成硼大环
2. Regiospecific synthesis of 1,2-aminoalcohol by ring-opening of racemic styrene oxide in presence of Lewis acids [J] . Abbes Boukhari, Rafika Blida, Fadhel Ismail Comptes Rendus Chimie . 2010,第12期

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5. Boronate macrocycle formation using boron-Lewis base dative bonds and boronic acid-diol condensation reactions. [D] . Rizzo, Natalie Rose. 2013

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机译：反式-1,2-二氟乙烯基双（膦酸）和其他不饱和膦酸的合成

Synthesis of boron macrocycles from 1,2-aminoalcohols and 2-formylphenylboronic acid

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