Synthesis and characterization of bis(mu-hydroxo)diiron(III) complex of N-(4-nitro-2-hydroxy)phenylmethyl-N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine and hydroxylation reaction of alkane.

Kurosaki H; Yoshida H; Ito M; Koike H; Higuchi E; Goto M

首页> 外文期刊>Bioorganic and Medicinal Chemistry Letters >Synthesis and characterization of bis(mu-hydroxo)diiron(III) complex of N-(4-nitro-2-hydroxy)phenylmethyl-N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine and hydroxylation reaction of alkane.

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Synthesis and characterization of bis(mu-hydroxo)diiron(III) complex of N-(4-nitro-2-hydroxy)phenylmethyl-N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine and hydroxylation reaction of alkane.

机译：N-（4-硝基-2-羟基）苯基甲基-N-（2-吡啶基乙基）-N-（2-吡啶基甲基）胺的双（mu-羟基-羟基）二铁（III）配合物的合成和表征以及烷烃的羟基化反应。

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摘要

Bis(mu-hydroxo)diiron(III) complex, [Fe2III(mu-OH)2(NE)2](NO3)2 x 3H2O (3) (N-(4-nitro-2-hydroxy)phenylmethyl-N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine = HNE, where H denotes a dissociable proton of the p-nitrophenol group), has been prepared and characterized by X-ray crystallography, electronic and magnetic spectroscopies.

机译：双（mu-hydroxo）二铁（III）络合物，[Fe2III（mu-OH）2（NE）2]（NO3）2 x 3H2O（3）（N-（4-硝基-2-羟基）苯基甲基-N-已经制备了（2-吡啶基乙基）-N-（2-吡啶基甲基）胺＝ HNE，其中H表示对硝基苯酚基团的可解离质子），并通过X射线晶体学，电子和磁光谱法进行了表征。

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来源
《Bioorganic and Medicinal Chemistry Letters》 |2001年第6期|共4页
作者
Kurosaki H; Yoshida H; Ito M; Koike H; Higuchi E; Goto M;
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正文语种 eng
中图分类药学;生物化学;
关键词
Alkanes; Ferric Compounds; Bis(mu hydroxo)diiron(III); N-(4-nitro-2-hydroxy)phenylmethyl N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine; 烷烃类; 正铁化合物;

机译：Alkanes;Ferric Compounds;Bis(mu hydroxo)diiron(III);N-(4-nitro-2-hydroxy)phenylmethyl N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine;烷烃类;正铁化合物;

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1. Synthesis and characterization of bis(mu-hydroxo)diiron(III) complex of N-(4-nitro-2-hydroxy)phenylmethyl-N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine and hydroxylation reaction of alkane. [J] . Kurosaki H, Yoshida H, Ito M, Bioorganic and Medicinal Chemistry Letters . 2001,第6期

机译：N-（4-硝基-2-羟基）苯基甲基-N-（2-吡啶基乙基）-N-（2-吡啶基甲基）胺的双（mu-羟基-羟基）二铁（III）配合物的合成和表征以及烷烃的羟基化反应。
2. Electrochemical synthesis and structural characterization of Co(II), Ni(II) and Cu(II) complexes of N,N-bis(4,5-dimethyl-2-hydroxybenzyl)-N-(2-pyridylmethyl)amine [J] . Labisbal E, Rodriguez L, Souto O, Dalton transactions: An international journal of inorganic chemistry . 2009,第40期

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机译：用N-（4-（二甲基氨基苄基）苯并D硫代-2-胺的一些过渡金属配合物的合成，表征和理论研究
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机译：第一部分：利塞膦酸盐双环类似物的不对称合成，作为双膦酸盐类抗骨质疏松药和潜在更有效的抗骨质疏松药作用机理的分子探针。第二部分使用Bestmann内酯从常见手性助剂轻松制备和官能化手性稳定化的叶基及其在Wittig反应中的用途。第三部分不对称有机催化：1.醛的α-羟基化研究； 2.合成新的基于樟脑的α-氨基四唑有机催化剂。
6. Bis-tridentate Chelates of an Asymmetric Ligand: X-ray Structures and Solution NMR Characterization of Divalent Zinc Triad Metal Ion Complexes of N-(2-pyridylmethyl)-N-(2-(methylthio)ethyl)amine [O] . Deborah C. Bebout, Wei Lai, Sarah M. Stamps, -1

机译：不对称配体的双三齿螯合物：N-（2-吡啶基甲基）-N-（2-（甲硫基）乙基）胺的二价锌三合会金属离子配合物的X射线结构和溶液NMR表征
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机译：（1,8）双（2-羟基苯苯甲酰氨基）（III）的形成动力学和机制，其与硫氰酸酯，叠氮化物，乙酸盐，硫（IV）和抗坏血酸在溶液中的反应，以及合成和合成新型氧代桥桥（III）复合物的表征。苯酚 - 酰胺 - 胺协调的作用

Synthesis and characterization of bis(mu-hydroxo)diiron(III) complex of N-(4-nitro-2-hydroxy)phenylmethyl-N-(2-pyridylethyl)-N-(2-pyridylmethyl)amine and hydroxylation reaction of alkane.

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