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Effect of Synthesis Temperature on the Morphology of ZnO Nanoparticies Obtained via a Novei Chemical Route

机译:合成温度对通过Novei化学路线获得的ZnO纳米颗粒形态的影响

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ZnO as a semiconductor is used in many applications such as gas sensor devices, laser and optoelectronic devices, photocatalysts, solar cells, and varistors. The applications and properties of ZnO nanoparticies highly depend on the size and morphology of these particles In this research ZnO nanoparticies were prepared via chemical bath deposition at various temperatures in order to see the effects of synthesis temperature and also 2-methoxyethanol (2-ME) as a novel solvent on the morphology of obtained nanoparticies. For synthesizing of ZnO nanostructured materials, 2-ME has been highly used in sol-gel process but it is the first time that it is used in the chemical bath deposition process. For this purpose 1 M solutions of zinc acetate dehydrate in 2-ME were prepared and added to the solution of NaOH in the same solvent dropwisely. Monoethanolamine (MEA) was used as surfactant The synthesis temperatures were 30°C, 60°C and 90°C. After filtering and drying, morphologies of obtained nanoparticies were characterized and compared.
机译:ZnO作为半导体用于许多应用中,例如气体传感器设备,激光和光电设备,光催化剂,太阳能电池和压敏电阻。 ZnO纳米颗粒的应用和性质高度取决于这些颗粒的大小和形态。在这项研究中,ZnO纳米颗粒是通过在不同温度下进行化学浴沉积制备的,目的是观察合成温度以及2-甲氧基乙醇(2-ME)的影响。作为获得纳米颗粒形态的新型溶剂。为了合成ZnO纳米结构材料,2-ME在溶胶-凝胶工艺中得到了广泛的应用,但这是它在化学浴沉积工艺中的首次应用。为此,制备1M乙酸锌脱水物在2-ME中的溶液,并将其滴加到相同溶剂中的NaOH溶液中。单乙醇胺(MEA)用作表面活性剂。合成温度为30℃,60℃和90℃。过滤并干燥后,对获得的纳米颗粒的形貌进行表征和比较。

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