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Statistical Parameters Effects on Photocatalytic Degradation of Rhodamine 6G Dye with Hexagonal Zinc Oxide Nanorods Synthesized via Solution Process

机译:统计参数对溶液法合成六方氧化锌纳米棒对罗丹明6G染料光催化降解的影响

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摘要

Hexagonal-shaped zinc oxide nanorods (HNRs) were synthesized via a wet chemical solution process at low temperature in short refluxing time. The structural and morphological properties of the obtained products were characterized by x-ray diffraction pattern and field emission scanning electron microscopy. The photocatalytic degradation process significantly shows enhanced activity of ZnO-HNRs under UV-Vis light in presence of rhodamine 6G dye (RhB). The effective concentration of ZnO-HNRs shows degradation process of RhB dye and was investigated via standard analytical techniques, optimized and validated by statistical analytical parameters. The statistical constraints give necessary information for establishing analytical procedures to ensure the quality and purity of the results. The absorption spectra were recorded at maximum absorbance lambda (max) 470 nm, 520 nm, and 550 nm for ZnO-HNRs, RhB and ZnO-HNRs-RhB, respectively. Satisfactory data were obtained from UV-Vis spectroscopy, providing more reliable values against many factual variable factors such as concentration, volume, pH, time and temperature, etc.
机译:通过低温湿法化学溶液法在短时间内回流合成了六边形的氧化锌纳米棒。通过X射线衍射图和场发射扫描电子显微镜对所得产物的结构和形态学性质进行表征。在罗丹明6G染料(RhB)的存在下,光催化降解过程显着显示ZnO-HNR在UV-Vis光下的活性增强。 ZnO-HNRs的有效浓度显示了RhB染料的降解过程,并通过标准分析技术进行了研究,并通过统计分析参数进行了优化和验证。统计约束条件为建立分析程序以确保结果的质量和纯度提供了必要的信息。分别在ZnO-HNRs,RhB和ZnO-HNRs-RhB的最大吸收λ(最大)470 nm,520 nm和550 nm处记录吸收光谱。从UV-Vis光谱学获得了令人满意的数据,针对许多事实可变因素(例如浓度,体积,pH,时间和温度等)提供了更可靠的值。

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