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High irradiance curing and anomalies of exposure reciprocity law in resin-based materials.

机译:树脂基材料的高辐照度固化和曝光互易法则异常。

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OBJECTIVES: The aim of this work was to investigate the effect of high irradiance curing on resultant degree of conversion of 'flowable' resin composites and their counterpart higher viscosity paste materials. METHODS: Five commercial flowable materials (Venus; Heraeus Kulzer, Synergy D6; Coltene, Premise; Kerr, Grandio; Voco and Gradia; GC Corp) and their counterpart higher viscosity restorative versions were tested. Specimens were cured with a halogen Swiss Master Light (EMS, Switzerland) using five different curing protocols with similar radiant exposure (18J/cm(2)): 400mW/cm(2) for 45s, 900mW/cm(2) for 20s, 1500mW/cm(2) for 12s, 2000mW/cm(2) for 9s and 3000mW/cm(2) for 6s. Degree of conversion (DC) was measured in real time by Fourier transform near infrared spectroscopy (FT-NIRS). RESULTS: Three- and subsequent two way ANOVA testing revealed significant differences (p
机译:目的:这项工作的目的是研究高辐照度固化对“可流动”树脂复合材料及其对应的更高粘度糊状材料转化率的影响。方法:测试了五种商用可流动材料(维纳斯; Heraeus Kulzer,Synergy D6;柯尔特尼,Premise; Kerr,Grandio; Voco和Gradia; GC Corp)及其对应的更高粘度的修复剂。使用五种不同的固化方案以类似的辐射暴露(18J / cm(2)):400mW / cm(2)持续45s,900mW / cm(2)持续20s,使用卤素瑞士万能灯(EMS,Switzerland)固化标本。 1500mW / cm(2)持续12s,2000mW / cm(2)持续9s和3000mW / cm(2)持续6s。通过傅立叶变换近红外光谱法(FT-NIRS)实时测量转化度(DC)。结果:在所有5种产品比较中,DC的“复合类型”和“固化方案”的三种方法以及随后的两种方差分析均显示出显着差异(p

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