Controlled-Potential Coulometric Determination of Ruthenium in Ru(OH)Cl_3 with Microwave Sample Preparation

N. A. Ezerskaya; E. S. Toropchenova; D. B. Pachgin; I. N. Kiseleva

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Controlled-Potential Coulometric Determination of Ruthenium in Ru(OH)Cl_3 with Microwave Sample Preparation

机译：微波前处理-电势库仑法测定Ru（OH）Cl_3中的钌

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A procedure for the controlled-potential coulometric (CPC) determination of ruthenium is proposed. The procedure is based on the redox reaction [Ru(CO)Cl_5]~(2_)/[Ru(CO)Cl_4(H2O)]~(2-) followed by the synthesis of the [Ru(CO)Cl_5]~(2-) depolarizing complex under microwave irradiation. The procedure was used in the analysis of a domestic commercial Ru(OH)Cl_3 preparation.

机译：提出了一种控制电位库仑法测定钌的方法。该程序基于氧化还原反应[Ru（CO）Cl_5]〜（2 _）/ [Ru（CO）Cl_4（H2O）]〜（2-），然后合成[Ru（CO）Cl_5]〜（ 2-）在微波辐射下使复合物去极化。该方法用于分析国内商业化Ru（OH）Cl_3制剂。

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《Journal of analytical chemistry》 |2004年第3期|共3页
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N. A. Ezerskaya; E. S. Toropchenova; D. B. Pachgin; I. N. Kiseleva;
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正文语种 eng
中图分类分析化学;
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1. Controlled-Potential Coulometric Determination of Ruthenium in Ru(OH)Cl_3 with Microwave Sample Preparation [J] . N. A. Ezerskaya, E. S. Toropchenova, D. B. Pachgin, Journal of analytical chemistry . 2004,第3期

机译：微波前处理-电势库仑法测定Ru（OH）Cl_3中的钌
2. Preparation of binuclear rhodium(II) tetraacetate (initial compound for the coulometric determination of Rhodium) under the action of microwave radiation [J] . N. A. Ezerskaya, E. S. Toropchenova, I. V. Kubrakova, Журнал аналитической химии . 2000,第12期

机译：微波辐射法制备双核四乙酸铑（II）（用于电量的库仑法测定的初始化合物）
3. Preparation of binuclear rhodium(II) tetraacetate (initial compound for the coulometric determination of Rhodium) under the action of microwave radiation [J] . N. A. Ezerskaya, E. S. Toropchenova, I. V. Kubrakova, Журнал аналитической химии . 2000,第12期

机译：微波辐射作用制备四核铑（II）四乙酸酯（用于库仑测定铑的初始化合物）
4. Determination of ruthenium in waste ruthenium catalysts using inductively coupled plasma optical emission spectrometry after sample digestion by high temperature fusion [C] . Jian Ming Pan, Xiao Juan Wei International Conference on Chemical Engineering and Advanced Materials . 2014

机译：高温融合后，使用电感耦合等离子体光发射光谱法测定废钌催化剂中的钌
5. Development of solventless sampling/sample preparation and introduction techniques for on-site determinations. [D] . Liu, Xin Yu. 2006

机译：开发无溶剂采样/样品制备和用于现场测定的引入技术。
6. Open focused microwave-assisted sample preparation for rapid total and mercury species determination in environmental solid samples [O] . C. M. Tseng, H. Garraud, D. Amouroux, 1998

机译：开放式聚焦微波辅助样品制备可快速测定环境固体样品中的总量和汞种类
7. Development of a microwave sample preparation method for the determination of arsenic in humus and moss samples by graphite furnace atomic absorption spectrometry [O] . Perämäki, P., Pesonen, M., Piispanen, J. 2000

机译：石墨炉原子吸收光谱法测定腐殖质和苔藓中砷的微波样品制备方法的建立
8. Automated Controlled-Potential Coulometric Determination of Uranium (Determination de l'Uranium par Coulometre Automatise a Potentiel Controle) [R] . Knight, C. H., Clegg, D. E., Wright, K. D., 1982

机译：自动控制电位库仑法测定铀（确定铀铀的自燃性自动控制铀）

Controlled-Potential Coulometric Determination of Ruthenium in Ru(OH)Cl_3 with Microwave Sample Preparation

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