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Carbon-nanotube-assisted transmission electron microscopy characterization of aerosol nanoparticles

机译:碳纳米管辅助的透射电子显微镜表征气溶胶纳米颗粒

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Aerosol nanoparticles draw great attention due to their unique physico-chemical properties that can be harnessed for innovative applications as well as for their potential impact on public health and the environment.Microscopic characterization of these particles is critically important to understand the unique particle properties and their interaction with biological systems.Here we report on a simple and efficient method for size,morphology,and crys-tallinity analyses of aerosol nanoparticles through transmission electron microscopy(TEM).The method uses carbon nanotubes(CNTs)as the particle support on conventional TEM grids.The CNT support significantly improves the quality of high resolution TEM(HRTEM)imaging due to the unique properties of CNTs,the high probability of particles sitting at the edge of CNTs,and the minimization of the interference interaction between the electron beam and the supporting substrate.The improved HRTEM images are useful for detailed characterization of nanoparticles,and particularly suitable for analyzing core-shell nanoparticles.
机译:气溶胶纳米颗粒由于其独特的物理化学特性可用于创新应用以及对公共健康和环境的潜在影响而备受关注。这些颗粒的微观表征对于理解独特的颗粒特性及其特性至关重要。我们在此报告了一种通过透射电子显微镜(TEM)对气溶胶纳米颗粒进行尺寸,形态和结晶度分析的简单有效方法。该方法使用碳纳米管(CNTs)作为常规TEM上的颗粒载体由于碳纳米管的独特性质,粒子位于碳纳米管边缘的可能性高以及将电子束与电子束之间的干扰相互作用最小化,碳纳米管支撑大大提高了高分辨率TEM(HRTEM)成像的质量。改进的HRTEM图像对于n的详细表征很有用纳米粒子,特别适合分析核壳纳米粒子。

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