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Grain Boundary Responses to Heterogeneous Deformation in Tantalum Polycrystals

机译:钽多晶对非均质形变的晶界响应

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The evolution of heterogeneous deformation in a tantalum polycrystal was examined during a three-point bending experiment using electron backscatter pattern mapping. Slip bands formed at strains as low as 1%, and they became more intense with strain. Heterogeneous deformation was evident as intra-granular orientation gradients as large as 30° were observed after a strain of about 8%. Nonmonotonic changes in the local average misorientation distribution were observed, implying that dislocation substructure developed in a complex manner. Slip bands were analyzed using plane traces computed from local orientation information. With the assumption of uniaxial stress, Schmid factors for favorable slip systems were identified for each grain and compared with observations, showing evidence for macroscopic activity on both {110} and {112} slip systems. Reconstructed boundary data were used to estimate the geometric potential for slip transfer at grain boundaries. The correlations indicated that when active slip systems were favorably oriented for slip transfer across the boundary, it was often observed in the form of continuous slip bands aligned across the boundary. In boundaries where geometrical alignment and Schmid factors were not favorable for slip transfer, there was a higher likelihood to form ledges (topographic discontinuities) along the grain boundaries. Dislocation pileups at grain boundaries were also correlated with a low potential for slip transfer.
机译:在三点弯曲实验中,使用电子背向散射谱图检查了钽多晶中非均质形变的演变。滑带在低至1%的应变下形成,并且随着应变而变得更强烈。异质变形是明显的,因为在约8%的应变后观察到的晶粒内取向梯度高达30°。观察到局部平均取向分布的非单调变化,这表明位错亚结构以复杂的方式发展。使用从局部方向信息计算的平面轨迹分析了滑带。在单轴应力的假设下,为每个晶粒确定了有利滑移系统的Schmid因子,并与观测值进行了比较,显示了{110}和{112}滑移系统宏观活动的证据。重建的边界数据被用来估计滑移在晶界的几何潜力。相关性表明,当主动滑移系统有利于滑移跨边界定向时,通常以跨边界对齐的连续滑移带的形式观察到。在几何排列和施密特因子不利于滑移的边界中,沿晶粒边界形成壁架(地形不连续)的可能性更高。晶界的位错堆积也与滑移的可能性低有关。

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