EFFICIENT SYNTHESIS OF FUNCTIONALIZED DIAZACYCLOPENTA[qPENTALENE WITH MULTIPLE INTERMOLECULAR INTERACTIONS IN CRYSTAL

Konstantin V. Kudryavtsev

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EFFICIENT SYNTHESIS OF FUNCTIONALIZED DIAZACYCLOPENTA[qPENTALENE WITH MULTIPLE INTERMOLECULAR INTERACTIONS IN CRYSTAL

机译：结晶中具有多个分子间相互作用的功能化二氮杂戊环戊四烯的高效合成

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Atom economic synthesis of functionalized polysubstituted racemic diazacyclopenta[c]pentalene 7 has been developed using sequential organocatalytic 1,3-dipolar cycloaddition of azomethine ylide with maleic anhydride and three successive amide bonds formation induced by interaction of 4-fluorobenzylamine with heterocyclic anhydride 5. Enantiomers of 7 are connected by Cl-π, H…F and C=O…H intermolecular interactions in crystal.

机译：利用偶氮甲胺与马来酸酐的顺序有机催化1,3-偶极环加成反应以及4-氟苄胺与杂环酸酐5的相互作用诱导的三个连续酰胺键的形成，已经开发了功能化多取代外消旋二氮杂环戊二烯[c]戊二烯的原子经济合成。 7个分子之间通过Cl-π，H…F和C = O…H在晶体中的分子间相互作用连接。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry 》 |2011年第2期| 共8页
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Konstantin V. Kudryavtsev;
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1. EFFICIENT SYNTHESIS OF FUNCTIONALIZED DIAZACYCLOPENTA[qPENTALENE WITH MULTIPLE INTERMOLECULAR INTERACTIONS IN CRYSTAL [J] . Konstantin V. Kudryavtsev Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2011 ,第2期

机译：结晶中具有多个分子间相互作用的功能化二氮杂戊环戊四烯的高效合成
2. Accurate and Efficient Model Energies for Exploring Intermolecular Interactions in Molecular Crystals [J] . Turner Michael J., Grabowsky Simon, Jayatilaka Dylan, Journal of physical chemistry letters . 2014 ,第24期

机译：探索分子晶体中分子间相互作用的准确高效的模型能量
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机译：取代的2,2'-联吡啶铅（II）壬基三氟丙酮酸铅（II）配合物的合成和晶体结构：晶体中分子间相互作用的相互作用。
4. Intermolecular interactions in molecular crystals studied by ab initio methods: From isolated interactions to patterns and crystals [C] . J.J.Novoa, NATO NATO advanced study institute on implications of molecular and materials structure for new technologies . 1999

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EFFICIENT SYNTHESIS OF FUNCTIONALIZED DIAZACYCLOPENTA[qPENTALENE WITH MULTIPLE INTERMOLECULAR INTERACTIONS IN CRYSTAL

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