SYNTHESIS, STRUCTURE AND ELECTROCHEMICAL BEHAVIOR OF A NOVEL REDOX-ACTIVE THIACALIX[4]ARENE-TETRATHIAFULVALENE ASSEMBLY

Bang-Tun Zhao; Wen-Bo Guo; Pu-Zhou Hu

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SYNTHESIS, STRUCTURE AND ELECTROCHEMICAL BEHAVIOR OF A NOVEL REDOX-ACTIVE THIACALIX[4]ARENE-TETRATHIAFULVALENE ASSEMBLY

机译：新型氧化还原活性噻唑烷[4]芳烃-四硫代富勒烯组件的合成，结构和电化学行为

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A novel redox-active thiacalix[4]arene-tetrathiafulvalene assembly 5 was carried out through triethyl phosphite-mediated cross-coupling of the corresponding two 1,3-dithiole-2-(thi)ones (3 and 4). The structure of thiacalix[4]arene-tetrathiafulvalene assembly 5 was identified by X-ray diffraction analysis. Meanwhile, the preliminary electrochemical properties of 5 was investigated by cyclic voltammetry (CV) and two one-electron quasi-reversible waves with redox potentials are observed.

机译：通过亚磷酸三乙酯介导的相应的两个1,3-二硫代-2-（thi）ones（3和4）的偶联反应，实现了一种新型的氧化还原活性的thiacalix [4] arene-ththiafulvalene组装体5。通过X射线衍射分析鉴定了硫杂杯[4]芳烃-四硫富瓦烯组件5的结构。同时，通过循环伏安法（CV）研究了5的初步电化学性质，并观察到两个具有氧化还原电势的单电子准可逆波。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2010年第7期|共7页
作者
Bang-Tun Zhao; Wen-Bo Guo; Pu-Zhou Hu;
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机译：新型氧化还原活性噻唑烷[4]芳烃-四硫代富勒烯组件的合成，结构和电化学行为
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机译：模型氧化还原活性硫杂杯4芳烃 - 四硫富瓦烯组装的合成和电化学行为

SYNTHESIS, STRUCTURE AND ELECTROCHEMICAL BEHAVIOR OF A NOVEL REDOX-ACTIVE THIACALIX[4]ARENE-TETRATHIAFULVALENE ASSEMBLY

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