Hexafluoroacetone as protecting and activating reagent:an efficient strategy for activation of pyroglutamic acid and homologues

Ksenia Pumpor; Christoph Bottcher; Susanna Fehn; Klaus Burger

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Hexafluoroacetone as protecting and activating reagent:an efficient strategy for activation of pyroglutamic acid and homologues

机译：六氟丙酮作为保护和活化剂：焦谷氨酸及其同系物活化的有效策略

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Hexafluoroacetone-protected glutamic acid to treatment with thionyl chloride is transformed into a carboxy-activated pyroglutamic acid derivative.Likewise,the reaction sequence can be applied to aminoadipic acid and homologues.

机译：用亚硫酰氯处理的六氟丙酮保护的谷氨酸被转化为羧基活化的焦谷氨酸衍生物。同样，该反应序列可应用于氨基己二酸和同系物。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2003年第1期|共11页
作者
Ksenia Pumpor; Christoph Bottcher; Susanna Fehn; Klaus Burger;
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正文语种 eng
中图分类杂环化合物;
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1. Hexafluoroacetone as protecting and activating reagent: an efficient strategy for activation of pyroglutamic acid and homologues [J] . Ksenia Pumpor, Christoph Bottcher, Susanna Fehn, Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2003,第0期

机译：六氟丙酮作为保护和活化剂：活化焦谷氨酸和同系物的有效策略
2. HEXAFLUOROACETONE AS ACTIVATING AND PROTECTING REAGENT IN AMINO ACID AND PEPTIDE CHEMISTRY .19. AN EFFICIENT APPROACH TO THE FAMILY OF 4-SUBSTITUTED PIPECOLIC ACIDS - SYNTHESES OF 4-OXO-, CIS-4-HYDROXY-, AND TRANS-4-HYDROXY-L-PIPECOLIC ACIDS FROM L-A [J] . Golubev A., Burger K., Sewald N. Tetrahedron letters: The International Journal for the Rapid Publication of Preliminary Communications in Organic Chemistry . 1995,第12期

机译：六氟丙酮作为氨基酸和肽化学中的活化和保护试剂.19。一种由4位取代的直链氨基酸组成的有效方法-由L-A合成4-OXO-，CIS-4-羟基-和反式-4-羟基-L-PI酸
3. Hexafluoroacetone as protecting and activating reagent:reactions of hexafluoroacetone with alpha-keto acids [J] . Jan Spengler, Sergej N.Osipov, Elisabeth Heistracher, Journal of Fluorine Chemistry . 2004,第6期

机译：六氟丙酮作为保护和活化剂：六氟丙酮与α-酮酸的反应
4. HEXAFLUOROACETONE AS A VERSATILE PROTECTING/ACTIVATING REAGENT FOR BETA-HYDROXY ACIDS, SERINE AND THREONINE [C] . Jan Spengler, Javier Ruiz-Rodriguez, Francesc Yraola the European Peptide Symposium . 2007

机译：六氟丙酮作为β-羟基酸，丝氨酸和苏氨酸的通用保护/活化试剂
5. Design of pH-controlled light-activated reagents for efficient cleavage of double-stranded DNA and cancer phototherapy. [D] . Yang, Wang-Yong. 2011

机译：pH控制的光活化试剂的设计，可有效裂解双链DNA和进行癌症光疗。
6. Michael Addition Reactions between Chiral Equivalents of a Nucleophilic Glycine and (S)- or (R)-3-(E)-Enoyl-4-phenyl-13-oxazolidin-2-ones as a General Method for Efficient Preparation of β-Substituted Pyroglutamic Acids. Case of Topographically Controlled Stereoselectivity [O] . Vadim A. Soloshonok*, Chaozhong Cai, Takeshi Yamada, -1

机译：亲核甘氨酸与（S）-或（R）-3-（E）-烯丙基 -4-苯基-13-恶唑烷-2-酮的手性当量之间的迈克尔加成反应作为有效制备的一般方法β-取代的焦谷氨酸地形控制立体选择性的情况
7. Application of hexafluoroacetone as protecting and activating reagent in solid phase peptide and depsipeptide synthesis [O] . Fernando Albericio, Klaus Burger, Tommaso Cupido, 2005

机译：六氟丙酮作为保护和活化试剂在固相肽和缩酚酸合成中的应用

Hexafluoroacetone as protecting and activating reagent:an efficient strategy for activation of pyroglutamic acid and homologues

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