9-ALKYLACRIDINE SYNTHESIS USING 2,2-DIMETHOXYPROPANE AS WATER SCAVENGER

George Bratulescu

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9-ALKYLACRIDINE SYNTHESIS USING 2,2-DIMETHOXYPROPANE AS WATER SCAVENGER

机译：2,2-二甲氧基丙烷作为除水剂合成9-烷基水素

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A rapid and high yielding green method was developed for acridine derivative synthesis in solvent free medium. The commercial reagents are easily converted into products by using of microwaves in a heterogeneous medium in the presence of zinc chloride and 2,2-dimethoxypropane. Principal advantages of the procedure are short time, low energy consumption, and easy work-up.

机译：开发了一种快速，高产率的绿色方法，用于在无溶剂介质中合成a啶衍生物。在氯化锌和2，2-二甲氧基丙烷的存在下，通过在异质介质中使用微波，可将商业试剂轻松转化为产物。该程序的主要优点是时间短，能耗低，后处理容易。

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《Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry》 |2014年第8期|共8页
作者
George Bratulescu;
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正文语种 eng
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1. 9-ALKYLACRIDINE SYNTHESIS USING 2,2-DIMETHOXYPROPANE AS WATER SCAVENGER [J] . George Bratulescu Heterocycles: An International Journal for Reviews and Communications in Heterocyclic Chemistry . 2014,第8期

机译：2,2-二甲氧基丙烷作为除水剂合成9-烷基水素
2. Use of 2,2-Dimethoxypropane and ~1H NMR To Distinguish and Quantify the External and Internal Sorbed Water in Coals [J] . Daniel A. Netzel, Thomas F. Turner, Francis P. Miknis, Energy & Fuels . 1996,第2期

机译：使用2,2-二甲氧基丙烷和〜1H NMR区分和量化煤中的外部和内部含盐水
3. A mixed Ni(II) ionic complex containing V-shaped water trimer: Synthesis, spectral, structural and thermal properties of {[Ni(2,2a€2-bpy)3][Ni(2-cpida)(2,2a€2 -bpy)]} (ClO4).3H2O [J] . Il-Shik Moon1, Kabali Senthilkumar, Mohan Gopalakrishnan, Journal of Chemical Sciences . 2015,第5期

机译：含V型三聚体的混合Ni（II）离子络合物：{[Ni（2,2a€2-bpy）3] [Ni（2-cpida）（2,2a€）的合成，光谱，结构和热性质2 -bpy）]}（ClO4）.3H2O
4. Simultaneous Quantitation of Five Leachables in Lipid Emulsions by LC-MS/MS Using 2,2-Dimethoxypropane as a De-emulsifying Reagent [C] . Yousheng Hua, James Story, Peifeng Hu, ASMS Conference on Mass Spectrometry and Allied Topics . 2016

机译：使用2,2-二甲氧基丙烷作为去乳化试剂，通过LC-MS / MS在脂质乳液中同时定量五种浸出物
5. Synthesis and Characterization of [Ru(tpyOH)(bpy)(H2O)][OTf]2 (tpyOH = 4′-Hydroxy-2,2’:6′, 2″- Terpyridine, Bpy = 2,2′-Bipyridine) for Water Oxidation Catalysis [D] . Isaacs, Diane Pearl. 2019

机译：[Ru（TPYOH）（BPY）（H2O）] [otf] 2（TPYOH = 4'-羟基-2,2'：6'，2“ - Terpyridine，BPy = 2,2'- Bi吡啶）的合成与表征用于水氧化催化
6. High yielding synthesis of 2,2′-bipyridine macrocycles, versatile intermediates in the synthesis of rotaxanes [O] . J. E. M. Lewis, R. J. Bordoli, M. Denis, 2018

机译：高产的2,2'-联吡啶大环化合物的合成，是轮烷的合成中的通用中间体
7. Novel Synthesis of Dienones and Enones from Propargyl Alcohols and Allyl Alcohols with 2,2-Dimethoxypropane: Synthesis of Ionone and Irone [O] . Toshinobu Ishihara, Takeshi Kitahara, Masanao Matsui 1974

机译：用2,2-二甲氧基丙烷的炔醇和烯丙醇和烯丙基醇的新颖合成：离子和虹膜的合成

9-ALKYLACRIDINE SYNTHESIS USING 2,2-DIMETHOXYPROPANE AS WATER SCAVENGER

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