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Purification of single-wall carbon nanotubes produced by arc plasma jet method

机译:电弧等离子体射流法制备单壁碳纳米管的纯化

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In the arc plasma jet method, a large amount of soot including single-wall carbon nanotubes (SWNTs) can be produced in a short time (1-2 g/ min). However, a lot of impurities, such as amorphous carbon and catalyst metals, are included in the produced soot besides SWNT. Purification is indispensable to apply SWNTs industrially, but it was difficult until recently. Here, we report that SWNTs can be purified easily in large quantities by reflux in the hydrogen peroxide solution using catalyst of iron particle, which can activate the oxidation reaction of hydrogen peroxide solution. Higher than 90 wt. percent purity of SWNTs are obtained by this technique.
机译:在电弧等离子体喷射方法中,可以在短时间内(1-2 g / min)产生大量的包括单壁碳纳米管(SWNT)在内的烟灰。但是,除SWNT外,生产的烟灰中还包含许多杂质,例如无定形碳和催化剂金属。纯化对于在工业上应用SWNT必不可少,但是直到最近还很难。在此,我们报道,SWNTs可以通过使用铁颗粒催化剂在过氧化氢溶液中回流而容易地大量纯化,这可以激活过氧化氢溶液的氧化反应。高于90 wt。通过该技术获得了100%SWNT的纯度。

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